5-cyclobutyl-2-[3-(N-2-nitrophenylsulfonyl-N-phenylmethyl)aminopropanoyl]-2,3-dihydro-[1H]-2-benzazepine

Base Information

Chemical Name:5-cyclobutyl-2-[3-(N-2-nitrophenylsulfonyl-N-phenylmethyl)aminopropanoyl]-2,3-dihydro-[1H]-2-benzazepine
CAS No.:1043927-54-3
Molecular Formula:C₃₀H₃₁N₃O₅S
Molecular Weight:545.659
Hs Code.:

Synonyms:5-cyclobutyl-2-[3-(N-2-nitrophenylsulfonyl-N-phenylmethyl)aminopropanoyl]-2,3-dihydro-[1H]-2-benzazepine

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Chemical Property of 5-cyclobutyl-2-[3-(N-2-nitrophenylsulfonyl-N-phenylmethyl)aminopropanoyl]-2,3-dihydro-[1H]-2-benzazepine

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Technology Process of 5-cyclobutyl-2-[3-(N-2-nitrophenylsulfonyl-N-phenylmethyl)aminopropanoyl]-2,3-dihydro-[1H]-2-benzazepine

There total 1 articles about 5-cyclobutyl-2-[3-(N-2-nitrophenylsulfonyl-N-phenylmethyl)aminopropanoyl]-2,3-dihydro-[1H]-2-benzazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1043871-02-8
3-(N-2-nitrophenylsulfonyl-N-phenylmethyl)aminopropanic acid

: 1043927-53-2
5-cyclobutyl-2,3-dihydro-[1H]-2-benzazepine

: 1043927-54-3
5-cyclobutyl-2-[3-(N-2-nitrophenylsulfonyl-N-phenylmethyl)aminopropanoyl]-2,3-dihydro-[1H]-2-benzazepine

Guidance literature:: 3-(N-2-nitrophenylsulfonyl-N-phenylmethyl)aminopropanic acid; With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 ℃; for 0.25h; Inert atmosphere;

5-cyclobutyl-2,3-dihydro-[1H]-2-benzazepine; In dichloromethane; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1039/b801206g