3,3'-dimethoxy-5,5'-dimethyl-[1,1'-biphenyl]-2,2'-diyl-O,O'-bis[5-methyl-2-(1-methylethyl)-cyclohexyl]-carbonic ester

Base Information

Chemical Name:3,3'-dimethoxy-5,5'-dimethyl-[1,1'-biphenyl]-2,2'-diyl-O,O'-bis[5-methyl-2-(1-methylethyl)-cyclohexyl]-carbonic ester
CAS No.:936102-23-7
Molecular Formula:C₃₈H₅₄O₈
Molecular Weight:638.842
Hs Code.:

Synonyms:3,3'-dimethoxy-5,5'-dimethyl-[1,1'-biphenyl]-2,2'-diyl-O,O'-bis[5-methyl-2-(1-methylethyl)-cyclohexyl]-carbonic ester

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Chemical Property of 3,3'-dimethoxy-5,5'-dimethyl-[1,1'-biphenyl]-2,2'-diyl-O,O'-bis[5-methyl-2-(1-methylethyl)-cyclohexyl]-carbonic ester

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Technology Process of 3,3'-dimethoxy-5,5'-dimethyl-[1,1'-biphenyl]-2,2'-diyl-O,O'-bis[5-methyl-2-(1-methylethyl)-cyclohexyl]-carbonic ester

There total 2 articles about 3,3'-dimethoxy-5,5'-dimethyl-[1,1'-biphenyl]-2,2'-diyl-O,O'-bis[5-methyl-2-(1-methylethyl)-cyclohexyl]-carbonic ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 13990-86-8
3,3'-dimethoxy-5,5'-dimethyl-[1,1'-biphenyl]-2,2'-diol

: 14602-86-9,7635-53-2
(1R,2S,5R)-menthyl chloroformate

: 936102-23-7
3,3'-dimethoxy-5,5'-dimethyl-[1,1'-biphenyl]-2,2'-diyl-O,O'-bis[5-methyl-2-(1-methylethyl)-cyclohexyl]-carbonic ester

Guidance literature:: With triethylamine; In toluene; at 20 ℃; for 1h;
DOI:10.1016/j.tetasy.2007.01.017

Reference yield:

: 93-51-6
2-Methoxy-4-methylphenol

: 936102-23-7
3,3'-dimethoxy-5,5'-dimethyl-[1,1'-biphenyl]-2,2'-diyl-O,O'-bis[5-methyl-2-(1-methylethyl)-cyclohexyl]-carbonic ester

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / methyltributylammonium permanganate / CH₂Cl₂ / 0 °C

2: 90 percent / triethylamine / toluene / 1 h / 20 °C

With methyltri(butyl)ammonium permanganate; triethylamine; In dichloromethane; toluene;
DOI:10.1016/j.tetasy.2007.01.017

Reference yield:

: 936102-23-7
3,3'-dimethoxy-5,5'-dimethyl-[1,1'-biphenyl]-2,2'-diyl-O,O'-bis[5-methyl-2-(1-methylethyl)-cyclohexyl]-carbonic ester

: 3,3'-dimethoxy-5,5'-dimethyl-6,6'-dibromo-[1,1'-biphenyl]-2,2'-diyl-O,O'-bis[5-methyl-2-(1-methylethyl)-cyclohexyl]-carbonic ester

: 3,3'-dimethoxy-5,5'-dimethyl-6,6'-dibromo-[1,1'-biphenyl]-2,2'-diyl-O,O'-bis[5-methyl-2-(1-methylethyl)-cyclohexyl]-carbonic ester

Guidance literature:: With acetic acid; benzyltriethylammonium tribromide; zinc(II) chloride; at 60 ℃; for 2h;
DOI:10.1016/j.tetasy.2007.01.017