Technology Process of C21H30O7
There total 6 articles about C21H30O7 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tetrabutyl ammonium fluoride;
In
tetrahydrofuran;
at 0 - 20 ℃;
for 1.5h;
Inert atmosphere;
DOI:10.1002/anie.201103270
- Guidance literature:
-
Multi-step reaction with 2 steps
1: magnesium bromide ethyl etherate / toluene / 1.17 h / -78 - 20 °C / Inert atmosphere
2: tetrabutyl ammonium fluoride / tetrahydrofuran / 1.5 h / 0 - 20 °C / Inert atmosphere
With
tetrabutyl ammonium fluoride; magnesium bromide ethyl etherate;
In
tetrahydrofuran; toluene;
1: Mukaiyama aldol reaction;
DOI:10.1002/anie.201103270
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / -78 - 0 °C / Inert atmosphere
1.2: 0.5 h / -78 °C / Inert atmosphere
2.1: osmium(VIII) oxide; (DHQ)2PYR; potassium carbonate; potassium hexacyanoferrate(III) / water; tert-butyl alcohol / 0 °C / Inert atmosphere
3.1: lead(IV) tetraacetate / dichloromethane / 0.75 h / Inert atmosphere
4.1: magnesium bromide ethyl etherate / toluene / 1.17 h / -78 - 20 °C / Inert atmosphere
5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1.5 h / 0 - 20 °C / Inert atmosphere
With
osmium(VIII) oxide; n-butyllithium; (DHQ)2PYR; tetrabutyl ammonium fluoride; lead(IV) tetraacetate; potassium carbonate; magnesium bromide ethyl etherate; potassium hexacyanoferrate(III);
In
tetrahydrofuran; hexane; dichloromethane; water; toluene; tert-butyl alcohol;
4.1: Mukaiyama aldol reaction;
DOI:10.1002/anie.201103270