[10,11-13C₂]-(2E,4E)-3-methyl-5-(2,6,6-trimethylcyclohex-1-enyl)penta-2,4-dienal

Base Information

• Chemical Name: [10,11-13C₂]-(2E,4E)-3-methyl-5-(2,6,6-trimethylcyclohex-1-enyl)penta-2,4-dienal
• CAS No.: 100187-26-6
• Molecular Formula: C₁₅H₂₂O
• Molecular Weight: 220.317

Synonyms:[10,11-13C₂]-(2E,4E)-3-methyl-5-(2,6,6-trimethylcyclohex-1-enyl)penta-2,4-dienal

Chemical Property of [10,11-13C₂]-(2E,4E)-3-methyl-5-(2,6,6-trimethylcyclohex-1-enyl)penta-2,4-dienal

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [10,11-13C₂]-(2E,4E)-3-methyl-5-(2,6,6-trimethylcyclohex-1-enyl)penta-2,4-dienal

There total 4 articles about [10,11-13C₂]-(2E,4E)-3-methyl-5-(2,6,6-trimethylcyclohex-1-enyl)penta-2,4-dienal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

C13(13)C2H24O (347367-54-8) → [10,11-13C2]-(2E,4E)-3-methyl-5-(2,6,6-trimethylcyclohex-1-enyl)penta-2,4-dienal (100187-26-6)

Guidance literature:

With manganese(IV) oxide; In hexane;

DOI:10.1002/jlcr.464

Reference yield:

(E)-β-ionone (79-77-6,14901-07-6) → [10,11-13C2]-(2E,4E)-3-methyl-5-(2,6,6-trimethylcyclohex-1-enyl)penta-2,4-dienal (100187-26-6)

Guidance literature:

Multi-step reaction with 3 steps

1: 99 percent / NaH / diethyl ether

2: 99 percent / LiAlH₄ / diethyl ether

3: 92 percent / MnO₂ / hexane

With manganese(IV) oxide; lithium aluminium tetrahydride; sodium hydride; In diethyl ether; hexane; 1: Wittig-Horner reaction;

DOI:10.1002/jlcr.464

Reference yield:

[10,11-13C2]-(2E,4E)-ethyl 3-methyl-5-(2,6,6-trimethylcyclohex-1-enyl)penta-2,4-dienoate (347367-53-7) → [10,11-13C2]-(2E,4E)-3-methyl-5-(2,6,6-trimethylcyclohex-1-enyl)penta-2,4-dienal (100187-26-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 99 percent / LiAlH₄ / diethyl ether

2: 92 percent / MnO₂ / hexane

With manganese(IV) oxide; lithium aluminium tetrahydride; In diethyl ether; hexane;

DOI:10.1002/jlcr.464

upstream raw materials:

C₁₃⁽¹³⁾C₂H₂₄O

(E)-β-ionone

[10,11-13C₂]-(2E,4E)-ethyl 3-methyl-5-(2,6,6-trimethylcyclohex-1-enyl)penta-2,4-dienoate

[10,11-13C₂]-(4E)-ethyl 3-methyl-5-(2,6,6-trimethylcyclohex-1-enyl)penta-2,4-dienoate

Downstream raw materials:

[10,11-13C₂]-((2E,6E,8E)-3,7-dimethyl-9-(2,6,6-trimethylcyclohex-1-enyl)nona-2,6,8-trien-4-ynyloxy)(tert-butyl)dimethylsilane

[10,11-13C₂]-1,3,3-trimethyl-2-((1E,3E)-3-methylhexa-1,3-dien-5-ynyl)cyclohex-1-ene

10,11,14,15-¹³C₄-retinoic acid ethyl ester

10,11,14,15-¹³C₄-retinol

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 100187-26-6 [10,11-13C₂]-(2E,4E)-3-methyl-5-(2,6,6-trimethylcyclohex-1-enyl)penta-2,4-dienal

Send

Send

Metric Ton KG G Pound L ML

Send

Send