Technology Process of C49H47N13O8S6
There total 9 articles about C49H47N13O8S6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
pyridine;
at 20 ℃;
for 0.166667h;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: formic acid
2: water; sodium hydroxide / tetrahydrofuran / 1.5 h / 60 °C
3: triethylamine / acetone / Sonication
4: sodium azide / acetone / 1.33 h / 60 °C
5: 14 h / 80 °C
6: dichloromethane / 0.5 h
7: pyridine; dmap / 0.17 h / 20 °C
With
pyridine; dmap; formic acid; sodium azide; water; triethylamine; sodium hydroxide;
In
tetrahydrofuran; dichloromethane; acetone;
5: Curtius rearrangement;
DOI:10.1021/jm101602q
- Guidance literature:
-
Multi-step reaction with 5 steps
1: triethylamine / acetone / Sonication
2: sodium azide / acetone / 1.33 h / 60 °C
3: 14 h / 80 °C
4: dichloromethane / 0.5 h
5: pyridine; dmap / 0.17 h / 20 °C
With
pyridine; dmap; sodium azide; triethylamine;
In
dichloromethane; acetone;
3: Curtius rearrangement;
DOI:10.1021/jm101602q