N-((1R,3S,5R)-6-benzyl-7-methylbicyclo[3.3.1]non-6-en-3-yl)hydroxylamine

Base Information

Chemical Name:N-((1R,3S,5R)-6-benzyl-7-methylbicyclo[3.3.1]non-6-en-3-yl)hydroxylamine
CAS No.:1146974-66-4
Molecular Formula:C₁₇H₂₃NO
Molecular Weight:257.376
Hs Code.:

Synonyms:N-((1R,3S,5R)-6-benzyl-7-methylbicyclo[3.3.1]non-6-en-3-yl)hydroxylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-((1R,3S,5R)-6-benzyl-7-methylbicyclo[3.3.1]non-6-en-3-yl)hydroxylamine

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Technology Process of N-((1R,3S,5R)-6-benzyl-7-methylbicyclo[3.3.1]non-6-en-3-yl)hydroxylamine

There total 4 articles about N-((1R,3S,5R)-6-benzyl-7-methylbicyclo[3.3.1]non-6-en-3-yl)hydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 1146974-65-3
(1R,5R)-6-benzyl-7-methylbicyclo[3.3.1]non-6-en-3-one oxime

: 1146974-66-4
N-((1R,3S,5R)-6-benzyl-7-methylbicyclo[3.3.1]non-6-en-3-yl)hydroxylamine

Guidance literature:: (1R,5R)-6-benzyl-7-methylbicyclo[3.3.1]non-6-en-3-one oxime; With ethanol; sodium cyanoborohydride; at 0 ℃; for 0.166667h; Inert atmosphere;

With trifluoroacetic acid; at 0 ℃; for 3h; Inert atmosphere;
DOI:10.1021/ol900441f

Reference yield:

: C₁₈H₂₄O₄S

: 1146974-66-4
N-((1R,3S,5R)-6-benzyl-7-methylbicyclo[3.3.1]non-6-en-3-yl)hydroxylamine

Guidance literature:: Multi-step reaction with 3 steps

1: silica gel / hexane / 10 h / Reflux; Inert atmosphere

2: pyridine; hydroxylamine hydrochloride / 3 h / 20 °C / Inert atmosphere

3: trifluoroacetic acid; sodium cyanoborohydride / ethanol / 3 h / 0 °C / Inert atmosphere

With pyridine; hydroxylamine hydrochloride; silica gel; sodium cyanoborohydride; trifluoroacetic acid; In ethanol; hexane;
DOI:10.1021/ja509766f

Reference yield:

: 1146974-64-2
(1R,5R)-6-benzyl-7-methylbicyclo[3.3.1]non-6-en-3-one

: 1146974-66-4
N-((1R,3S,5R)-6-benzyl-7-methylbicyclo[3.3.1]non-6-en-3-yl)hydroxylamine

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine; hydroxylamine hydrochloride / 3 h / 20 °C / Inert atmosphere

2: trifluoroacetic acid; sodium cyanoborohydride / ethanol / 3 h / 0 °C / Inert atmosphere

With pyridine; hydroxylamine hydrochloride; sodium cyanoborohydride; trifluoroacetic acid; In ethanol;
DOI:10.1021/ja509766f