Technology Process of C19H17N5O6
There total 6 articles about C19H17N5O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
triethylamine;
In
tetrahydrofuran;
at 20 ℃;
for 3h;
Inert atmosphere;
DOI:10.1021/jm301097p
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 5%-palladium/activated carbon; hydrogen / ethanol / 2 h / 760.05 Torr
2: benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide; tetrahydrofuran / 20 °C / Inert atmosphere
3: triethylamine / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere
With
5%-palladium/activated carbon; hydrogen; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm301097p
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sulfuric acid / 6 h / Reflux
2: 5%-palladium/activated carbon; hydrogen / ethanol / 2 h / 760.05 Torr
3: benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide; tetrahydrofuran / 20 °C / Inert atmosphere
4: triethylamine / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere
With
sulfuric acid; 5%-palladium/activated carbon; hydrogen; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm301097p
