8,10-bis(p-methoxybenzyl)-8,10-diaza-1-<2'-methyl-1'-hydroxy-2',3'-(isopropylidenedioxy)propyl>-2-oxabicyclo<4.2.2>decane-7,9-dione

Base Information

• Chemical Name: 8,10-bis(p-methoxybenzyl)-8,10-diaza-1-<2'-methyl-1'-hydroxy-2',3'-(isopropylidenedioxy)propyl>-2-oxabicyclo<4.2.2>decane-7,9-dione
• CAS No.: 96000-08-7
• Molecular Formula: C₃₀H₃₈N₂O₈
• Molecular Weight: 554.64

Synonyms:8,10-bis(p-methoxybenzyl)-8,10-diaza-1-<2'-methyl-1'-hydroxy-2',3'-(isopropylidenedioxy)propyl>-2-oxabicyclo<4.2.2>decane-7,9-dione

Chemical Property of 8,10-bis(p-methoxybenzyl)-8,10-diaza-1-<2'-methyl-1'-hydroxy-2',3'-(isopropylidenedioxy)propyl>-2-oxabicyclo<4.2.2>decane-7,9-dione

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Technology Process of 8,10-bis(p-methoxybenzyl)-8,10-diaza-1-<2'-methyl-1'-hydroxy-2',3'-(isopropylidenedioxy)propyl>-2-oxabicyclo<4.2.2>decane-7,9-dione

There total 2 articles about 8,10-bis(p-methoxybenzyl)-8,10-diaza-1-<2'-methyl-1'-hydroxy-2',3'-(isopropylidenedioxy)propyl>-2-oxabicyclo<4.2.2>decane-7,9-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(+/-)-2,2,4-trimethyl-1,3-dioxolane-4-carboxaldehyde (81600-36-4) + 8,10-bis(p-methoxybenzyl)-8,10-diaza-2-oxabicyclo<4.2.2>decane-7,9-dione (91238-09-4,95999-81-8) → 8,10-bis(p-methoxybenzyl)-8,10-diaza-1-<2'-methyl-1'-hydroxy-2',3'-(isopropylidenedioxy)propyl>-2-oxabicyclo<4.2.2>decane-7,9-dione (96000-08-7) + 8,10-bis(p-methoxybenzyl)-8,10-diaza-1-<2'-methyl-1'-hydroxy-2',3'-(isopropylidenedioxy)propyl>-2-oxabicyclo<4.2.2>decane-7,9-dione (96000-08-7)

Guidance literature:

Yield given. Multistep reaction. Yields of byproduct given;

DOI:10.1021/jm00383a008

Reference yield:

(+/-)-2,2,4-trimethyl-1,3-dioxolane-4-carboxaldehyde (81600-36-4) + 8,10-bis(p-methoxybenzyl)-8,10-diaza-2-oxabicyclo<4.2.2>decane-7,9-dione (91238-09-4,95999-81-8) → 8,10-bis(p-methoxybenzyl)-8,10-diaza-1-<2'-methyl-1'-hydroxy-2',3'-(isopropylidenedioxy)propyl>-2-oxabicyclo<4.2.2>decane-7,9-dione (96000-08-7) + 8,10-bis(p-methoxybenzyl)-8,10-diaza-1-<2'-methyl-1'-hydroxy-2',3'-(isopropylidenedioxy)propyl>-2-oxabicyclo<4.2.2>decane-7,9-dione (96000-08-7)

Guidance literature:

Yield given. Multistep reaction. Yields of byproduct given;

DOI:10.1021/jm00383a008

Reference yield: 72.0%

8,10-bis(p-methoxybenzyl)-8,10-diaza-1-<2'-methyl-1'-hydroxy-2',3'-(isopropylidenedioxy)propyl>-2-oxabicyclo<4.2.2>decane-7,9-dione (96000-08-7) + trifluoroacetic anhydride (407-25-0) → Trifluoro-acetic acid (2R,3R)-3-[(1R,6R)-7,9-bis-(4-methoxy-benzyl)-8,10-dioxo-2-oxa-7,9-diaza-bicyclo[4.2.2]dec-1-yl]-2,3-dihydroxy-2-methyl-propyl ester

Guidance literature:

With dmap; In dichloromethane; for 2h; Ambient temperature;

DOI:10.1021/jm00383a008

upstream raw materials:

(+/-)-2,2,4-trimethyl-1,3-dioxolane-4-carboxaldehyde

8,10-bis(p-methoxybenzyl)-8,10-diaza-2-oxabicyclo<4.2.2>decane-7,9-dione

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