C₆₃H₈₄Cl₃N₅O₁₃S

Base Information

Chemical Name:C₆₃H₈₄Cl₃N₅O₁₃S
CAS No.:1239985-37-5
Molecular Formula:C₆₃H₈₄Cl₃N₅O₁₃S
Molecular Weight:1257.81
Hs Code.:

C<sub>63</sub>H<sub>84</sub>Cl<sub>3</sub>N<sub>5</sub>O<sub>13</sub>S

Synonyms:C₆₃H₈₄Cl₃N₅O₁₃S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₆₃H₈₄Cl₃N₅O₁₃S

Chemical Property:

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Technology Process of C₆₃H₈₄Cl₃N₅O₁₃S

There total 12 articles about C₆₃H₈₄Cl₃N₅O₁₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1352449-74-1
C₄₅H₆₉Cl₃N₄O₁₀S

: 35661-38-2,35661-39-3,79990-15-1,136132-75-7
N-(9-fluorenylmethoxycarbonyl)-D-alanine

: 1239985-37-5
C₆₃H₈₄Cl₃N₅O₁₃S

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 0 - 20 ℃; for 4h;
DOI:10.1016/j.tet.2011.10.094

Reference yield:

: 1204215-22-4
C₈H₁₄Cl₃NO₂*ClH

: 1239985-37-5
C₆₃H₈₄Cl₃N₅O₁₃S

Guidance literature:: Multi-step reaction with 10 steps

1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane; N,N-dimethyl-formamide / 6 h / 20 °C

2: hydrogenchloride / 1,4-dioxane / 1 h / 10 - 15 °C

3: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane; N,N-dimethyl-formamide / 12 h / 20 °C

4: hydrogenchloride / 1,4-dioxane / 1 h / 0 °C

5: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; triethylamine; N-ethyl-N,N-diisopropylamine / dichloromethane; N,N-dimethyl-formamide / 22 h

6: hydrogenchloride / 1,4-dioxane

7: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane; N,N-dimethyl-formamide / 25 h

8: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 12 h

9: pyridine hydrogenfluoride

10: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 4 h / 0 - 20 °C

With hydrogenchloride; dmap; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; pyridine hydrogenfluoride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2011.10.094

Reference yield:

: 1239981-42-0
C₁₃H₂₂Cl₃NO₄

: 1239985-37-5
C₆₃H₈₄Cl₃N₅O₁₃S

Guidance literature:: Multi-step reaction with 11 steps

1: hydrogenchloride / 1,4-dioxane / 2 h / 20 °C

2: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane; N,N-dimethyl-formamide / 6 h / 20 °C

3: hydrogenchloride / 1,4-dioxane / 1 h / 10 - 15 °C

4: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane; N,N-dimethyl-formamide / 12 h / 20 °C

5: hydrogenchloride / 1,4-dioxane / 1 h / 0 °C

6: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; triethylamine; N-ethyl-N,N-diisopropylamine / dichloromethane; N,N-dimethyl-formamide / 22 h

7: hydrogenchloride / 1,4-dioxane

8: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane; N,N-dimethyl-formamide / 25 h

9: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 12 h

10: pyridine hydrogenfluoride

11: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 4 h / 0 - 20 °C

With hydrogenchloride; dmap; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; pyridine hydrogenfluoride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2011.10.094