N-[5-Bromo-3,4-dicyano-1-(4-methyl-benzyl)-1H-pyrrol-2-yl]-formimidic acid ethyl ester

Base Information

Chemical Name:N-[5-Bromo-3,4-dicyano-1-(4-methyl-benzyl)-1H-pyrrol-2-yl]-formimidic acid ethyl ester
CAS No.:1026173-84-1
Molecular Formula:C₁₇H₁₅BrN₄O
Molecular Weight:371.236
Hs Code.:

Synonyms:N-[5-Bromo-3,4-dicyano-1-(4-methyl-benzyl)-1H-pyrrol-2-yl]-formimidic acid ethyl ester

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Chemical Property of N-[5-Bromo-3,4-dicyano-1-(4-methyl-benzyl)-1H-pyrrol-2-yl]-formimidic acid ethyl ester

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Technology Process of N-[5-Bromo-3,4-dicyano-1-(4-methyl-benzyl)-1H-pyrrol-2-yl]-formimidic acid ethyl ester

There total 2 articles about N-[5-Bromo-3,4-dicyano-1-(4-methyl-benzyl)-1H-pyrrol-2-yl]-formimidic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 98130-58-6
2-amino-5-bromo-1H-pyrrole-3,4-dicarbonitrile

: 1026173-84-1
N-[5-Bromo-3,4-dicyano-1-(4-methyl-benzyl)-1H-pyrrol-2-yl]-formimidic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: acetonitrile / 2.5 h / Heating

2: 1.) NaH / 1.) acetonitrile, RT, 0.5 h, 2.) acetonitrile, RT, 30 min

With sodium hydride; In acetonitrile;
DOI:10.1021/jm950444j

Reference yield:

: N-(5-Bromo-3,4-dicyano-1H-pyrrol-2-yl)-formimidic acid ethyl ester

: 1026173-84-1
N-[5-Bromo-3,4-dicyano-1-(4-methyl-benzyl)-1H-pyrrol-2-yl]-formimidic acid ethyl ester

Guidance literature:: With sodium hydride; Multistep reaction; 1.) acetonitrile, RT, 0.5 h, 2.) acetonitrile, RT, 30 min;
DOI:10.1021/jm950444j

Reference yield:

: 1026173-84-1
N-[5-Bromo-3,4-dicyano-1-(4-methyl-benzyl)-1H-pyrrol-2-yl]-formimidic acid ethyl ester

: 172043-39-9
4-amino-7-(4-methylbenzyl)-pyrrolo[2,3-d]pyrimidine-5-carbonitryle

Guidance literature:: Multi-step reaction with 2 steps

1: NH₃ / methanol / 24 h / Ambient temperature

2: 81 percent / H₂, 1N aq. NaOH / 10percent Pd/C / ethyl acetate; ethanol / 0.5 h / 2585.7 Torr / Ambient temperature

With sodium hydroxide; ammonia; hydrogen; palladium on activated charcoal; In methanol; ethanol; ethyl acetate;
DOI:10.1021/jm950444j