methyl -phenylalaninate

Base Information

Chemical Name:methyl -phenylalaninate
CAS No.:147715-90-0
Molecular Formula:C₁₇H₂₀N₂O₄S
Molecular Weight:348.423
Hs Code.:

methyl <N-(N'-benzyl)-sulfamoyl>-phenylalaninate

Synonyms:methyl -phenylalaninate

Suppliers and Price of methyl -phenylalaninate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl -phenylalaninate

Chemical Property:

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Technology Process of methyl -phenylalaninate

There total 4 articles about methyl -phenylalaninate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 147715-89-7
<(S)(+)> methyl -phenylalaninate

: 147715-90-0
methyl -phenylalaninate

Guidance literature:: With trifluoroacetic acid; In dichloromethane; for 2h;
DOI:10.1016/0040-4020(95)00932-9

Reference yield:

: 7524-50-7
methyl (2S)-2-amino-3-phenylpropanoate hydrochloride

: 147715-90-0
methyl -phenylalaninate

Guidance literature:: Multi-step reaction with 3 steps

1: 2.) Et₃N

2: 95 percent / diethylazodicarboxylate, PPh₃ / tetrahydrofuran / 0.75 h / 5 °C

3: 92 percent / TFA / CH₂Cl₂ / 2 h

With triethylamine; triphenylphosphine; trifluoroacetic acid; diethylazodicarboxylate; In tetrahydrofuran; dichloromethane;
DOI:10.1016/0040-4020(95)00932-9

Reference yield:

: 139059-69-1
<(S)(+)> methyl -phenylalaninate

: 147715-90-0
methyl -phenylalaninate

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / diethylazodicarboxylate, PPh₃ / tetrahydrofuran / 0.75 h / 5 °C

2: 92 percent / TFA / CH₂Cl₂ / 2 h

With triphenylphosphine; trifluoroacetic acid; diethylazodicarboxylate; In tetrahydrofuran; dichloromethane;
DOI:10.1016/0040-4020(95)00932-9