2-methyl-2-phenylbutanoyl azide

Base Information

Chemical Name:2-methyl-2-phenylbutanoyl azide
CAS No.:1195178-92-7
Molecular Formula:C₁₁H₁₃N₃O
Molecular Weight:203.244
Hs Code.:

Synonyms:2-methyl-2-phenylbutanoyl azide

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Chemical Property of 2-methyl-2-phenylbutanoyl azide

Chemical Property:

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Technology Process of 2-methyl-2-phenylbutanoyl azide

There total 2 articles about 2-methyl-2-phenylbutanoyl azide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 51018-80-5
2-methyl-2-phenylbutanoic acid

: 1195178-92-7
2-methyl-2-phenylbutanoyl azide

Guidance literature:: 2-methyl-2-phenylbutanoic acid; With chloroformic acid ethyl ester; triethylamine; In tetrahydrofuran; at 0 - 20 ℃;

With sodium azide; In tetrahydrofuran; water; at 20 ℃;

Reference yield:

: 769-68-6
2-phenylbutanenitrile

: 1195178-92-7
2-methyl-2-phenylbutanoyl azide

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hexamethyldisilazane / tetrahydrofuran; toluene / 0 - 20 °C

2.1: hydrogenchloride; water / 2 h / 150 °C / microwave irradiation

3.1: chloroformic acid ethyl ester; triethylamine / tetrahydrofuran / 0 - 20 °C

3.2: 20 °C

With hydrogenchloride; water; sodium hexamethyldisilazane; chloroformic acid ethyl ester; triethylamine; In tetrahydrofuran; toluene;

Reference yield:

: 216059-91-5
4-(2-methylpyridin-4-yl)phenylamine

: 1195178-92-7
2-methyl-2-phenylbutanoyl azide

: 1195173-39-7
1-(4-(2-methylpyridin-4-yl)phenyl)-3-(2-phenylbutan-2-yl)urea

Guidance literature:: 2-methyl-2-phenylbutanoyl azide; In tetrahydrofuran; at 130 ℃; for 0.25h; microwave irradiation;

4-(2-methylpyridin-4-yl)phenylamine; In tetrahydrofuran; at 130 ℃; for 0.25h; microwave irradiation;