4-amino-6-bromo-7-(3-methylbenzyl)-pyrrolo[2,3-d]pyrimidine-5-carbonitryle

Base Information

Chemical Name:4-amino-6-bromo-7-(3-methylbenzyl)-pyrrolo[2,3-d]pyrimidine-5-carbonitryle
CAS No.:172043-33-3
Molecular Formula:C₁₅H₁₂BrN₅
Molecular Weight:342.198
Hs Code.:

Synonyms:4-amino-6-bromo-7-(3-methylbenzyl)-pyrrolo[2,3-d]pyrimidine-5-carbonitryle

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Chemical Property of 4-amino-6-bromo-7-(3-methylbenzyl)-pyrrolo[2,3-d]pyrimidine-5-carbonitryle

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Technology Process of 4-amino-6-bromo-7-(3-methylbenzyl)-pyrrolo[2,3-d]pyrimidine-5-carbonitryle

There total 3 articles about 4-amino-6-bromo-7-(3-methylbenzyl)-pyrrolo[2,3-d]pyrimidine-5-carbonitryle which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1026279-90-2
N-[5-Bromo-3,4-dicyano-1-(3-methyl-benzyl)-1H-pyrrol-2-yl]-formimidic acid ethyl ester

: 172043-33-3
4-amino-6-bromo-7-(3-methylbenzyl)-pyrrolo[2,3-d]pyrimidine-5-carbonitryle

Guidance literature:: With ammonia; In methanol; for 24h; Yield given; Ambient temperature;
DOI:10.1021/jm950444j

Reference yield:

: 98130-58-6
2-amino-5-bromo-1H-pyrrole-3,4-dicarbonitrile

: 172043-33-3
4-amino-6-bromo-7-(3-methylbenzyl)-pyrrolo[2,3-d]pyrimidine-5-carbonitryle

Guidance literature:: Multi-step reaction with 3 steps

1: acetonitrile / 2.5 h / Heating

2: 1.) NaH / 1.) acetonitrile, RT, 0.5 h, 2.) acetonitrile, RT, 30 min

3: NH₃ / methanol / 24 h / Ambient temperature

With ammonia; sodium hydride; In methanol; acetonitrile;
DOI:10.1021/jm950444j

Reference yield:

: N-(5-Bromo-3,4-dicyano-1H-pyrrol-2-yl)-formimidic acid ethyl ester

: 172043-33-3
4-amino-6-bromo-7-(3-methylbenzyl)-pyrrolo[2,3-d]pyrimidine-5-carbonitryle

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) acetonitrile, RT, 0.5 h, 2.) acetonitrile, RT, 30 min

2: NH₃ / methanol / 24 h / Ambient temperature

With ammonia; sodium hydride; In methanol;
DOI:10.1021/jm950444j