C₅₂H₄₀Br₂S₇

Base Information

• Chemical Name: C₅₂H₄₀Br₂S₇
• CAS No.: 1443155-54-1
• Molecular Formula: C₅₂H₄₀Br₂S₇
• Molecular Weight: 1049.16
• Mol file: 1443155-54-1.mol

Synonyms:C₅₂H₄₀Br₂S₇

Chemical Property of C₅₂H₄₀Br₂S₇

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of C₅₂H₄₀Br₂S₇

There total 1 articles about C₅₂H₄₀Br₂S₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

1,3,5-trisbromobenzene (626-39-1) + 3,5-Bis-(3,5-bis-p-tolylsulfanyl-phenylsulfanyl)-benzenethiol → C52H40Br2S7 (1443155-54-1)

Guidance literature:

3,5-Bis-(3,5-bis-p-tolylsulfanyl-phenylsulfanyl)-benzenethiol; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 0.166667h; Inert atmosphere; Schlenk technique;

1,3,5-trisbromobenzene; In N,N-dimethyl-formamide; at 80 ℃; for 12h; Inert atmosphere;

DOI:10.1016/j.tet.2013.04.058

Reference yield: 67.0%

C52H40Br2S7 (1443155-54-1) + 4-ethynylpyridine hydrochloride → C66H48N2S7 (1443155-57-4)

Guidance literature:

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; diisopropylamine; In tetrahydrofuran; at 65 ℃; for 12h; Inert atmosphere; Schlenk technique;

DOI:10.1016/j.tet.2013.04.058

upstream raw materials:

1,3,5-trisbromobenzene

Downstream raw materials:

C₆₆H₄₈N₂S₇