Technology Process of C28H29NO5
There total 4 articles about C28H29NO5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
water; sodium hydroxide;
In
methanol;
at 60 ℃;
for 0.5h;
Inert atmosphere;
DOI:10.1016/j.bmc.2012.12.002
- Guidance literature:
-
Multi-step reaction with 5 steps
1: pyridine / dichloromethane / 3 h / 20 °C
2: trifluoromethylsulfonic anhydride / dichloromethane / 15 h / 20 °C
3: boron trichloride / dichloromethane / 72 h / 0 - 20 °C
4: triethylsilane; trifluoroacetic acid / dichloromethane / 20 °C
5: water; sodium hydroxide / methanol / 0.5 h / 60 °C / Inert atmosphere
With
pyridine; triethylsilane; trifluoromethylsulfonic anhydride; water; boron trichloride; trifluoroacetic acid; sodium hydroxide;
In
methanol; dichloromethane;
2: |Friedel-Crafts Acylation;
DOI:10.1016/j.bmc.2012.12.002
- Guidance literature:
-
Multi-step reaction with 7 steps
1: copper; triethylamine / dichloromethane / 120 h / 20 °C
2: palladium 10% on activated carbon; hydrogen / ethyl acetate / 20 °C
3: pyridine / dichloromethane / 3 h / 20 °C
4: trifluoromethylsulfonic anhydride / dichloromethane / 15 h / 20 °C
5: boron trichloride / dichloromethane / 72 h / 0 - 20 °C
6: triethylsilane; trifluoroacetic acid / dichloromethane / 20 °C
7: water; sodium hydroxide / methanol / 0.5 h / 60 °C / Inert atmosphere
With
pyridine; triethylsilane; trifluoromethylsulfonic anhydride; palladium 10% on activated carbon; water; hydrogen; boron trichloride; copper; triethylamine; trifluoroacetic acid; sodium hydroxide;
In
methanol; dichloromethane; ethyl acetate;
4: |Friedel-Crafts Acylation;
DOI:10.1016/j.bmc.2012.12.002
