(benzotriazol-1-yl)diethoxymethane

Base Information

• Chemical Name: (benzotriazol-1-yl)diethoxymethane
• CAS No.: 161806-75-3
• Molecular Formula: C₁₁H₁₅N₃O₂
• Molecular Weight: 221.259
• Mol file: 161806-75-3.mol

Synonyms:(benzotriazol-1-yl)diethoxymethane

Chemical Property of (benzotriazol-1-yl)diethoxymethane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (benzotriazol-1-yl)diethoxymethane

There total 1 articles about (benzotriazol-1-yl)diethoxymethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

1,2,3-Benzotriazole (95-14-7,27556-51-0) + orthoformic acid triethyl ester (122-51-0) → 1-ethylbenzotriazole (16584-05-7) + (benzotriazol-1-yl)diethoxymethane (161806-75-3)

Guidance literature:

In various solvent(s); for 20h; Heating;

DOI:10.1021/jo9612335

Reference yield: 95.0%

(benzotriazol-1-yl)diethoxymethane (161806-75-3) + C20H20Al(1-)*Na(1+) → phenylpropargyl aldehyde diethyl acetal (6142-95-6)

Guidance literature:

With zinc(II) iodide; In diethyl ether; toluene; for 1h; Ambient temperature;

DOI:10.1021/jo9814750

Reference yield: 90.0%

(benzotriazol-1-yl)diethoxymethane (161806-75-3) + C14H28AlSi2(1-)*Na(1+) → 1,1-diethoxy-3-(trimethylsilyl)prop-2-yne (87219-80-5)

Guidance literature:

With zinc(II) iodide; In diethyl ether; toluene; for 1h; Ambient temperature;

DOI:10.1021/jo9814750

upstream raw materials:

1,2,3-Benzotriazole

orthoformic acid triethyl ester

Downstream raw materials:

phenylpropargyl aldehyde diethyl acetal

1,1-diethoxy-3-(trimethylsilyl)prop-2-yne

1,1-diethoxy-2-octyne

1-phenyl-1,3,3-triethoxypropane