benzyl 4-[(tert-Butoxycarbonyl)(methyl)amino]-2-(hydroxymethyl)piperidine-1-carboxylate

Base Information

Chemical Name:benzyl 4-[(tert-Butoxycarbonyl)(methyl)amino]-2-(hydroxymethyl)piperidine-1-carboxylate
CAS No.:845256-73-7
Molecular Formula:C₂₀H₃₀N₂O₅
Molecular Weight:378.469
Hs Code.:

Synonyms:benzyl 4-[(tert-Butoxycarbonyl)(methyl)amino]-2-(hydroxymethyl)piperidine-1-carboxylate

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Chemical Property of benzyl 4-[(tert-Butoxycarbonyl)(methyl)amino]-2-(hydroxymethyl)piperidine-1-carboxylate

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Technology Process of benzyl 4-[(tert-Butoxycarbonyl)(methyl)amino]-2-(hydroxymethyl)piperidine-1-carboxylate

There total 4 articles about benzyl 4-[(tert-Butoxycarbonyl)(methyl)amino]-2-(hydroxymethyl)piperidine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₁H₃₀N₂O₆

: 845256-73-7
benzyl 4-[(tert-Butoxycarbonyl)(methyl)amino]-2-(hydroxymethyl)piperidine-1-carboxylate

Guidance literature:: With lithium borohydride; In tetrahydrofuran; methanol; at 0 - 20 ℃;

Reference yield:

: 847029-99-6,1357348-22-1
1-benzyl 2-methyl 4-hydroxypiperidine-1,2-dicarboxylate

: 845256-73-7
benzyl 4-[(tert-Butoxycarbonyl)(methyl)amino]-2-(hydroxymethyl)piperidine-1-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / dichloromethane / 5 h / 20 °C

2: acetic acid / methanol / 1 h

3: triethylamine / dichloromethane / 72 h

4: lithium borohydride / tetrahydrofuran; methanol / 0 - 20 °C

With lithium borohydride; sulfur trioxide pyridine complex; acetic acid; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; methanol; dichloromethane;

Reference yield:

: C₁₆H₂₂N₂O₄

: 845256-73-7
benzyl 4-[(tert-Butoxycarbonyl)(methyl)amino]-2-(hydroxymethyl)piperidine-1-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 72 h

2: lithium borohydride / tetrahydrofuran; methanol / 0 - 20 °C

With lithium borohydride; triethylamine; In tetrahydrofuran; methanol; dichloromethane;