N-(methoxycarbonylmethyl)-N'-[(2'S)-1,2-bis(benzyloxycarbonyl)ethyl]sulfamide

Base Information

Chemical Name:N-(methoxycarbonylmethyl)-N'-[(2'S)-1,2-bis(benzyloxycarbonyl)ethyl]sulfamide
CAS No.:249538-99-6
Molecular Formula:C₂₁H₂₄N₂O₈S
Molecular Weight:464.496
Hs Code.:

Synonyms:N-(methoxycarbonylmethyl)-N'-[(2'S)-1,2-bis(benzyloxycarbonyl)ethyl]sulfamide

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Chemical Property of N-(methoxycarbonylmethyl)-N'-[(2'S)-1,2-bis(benzyloxycarbonyl)ethyl]sulfamide

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Technology Process of N-(methoxycarbonylmethyl)-N'-[(2'S)-1,2-bis(benzyloxycarbonyl)ethyl]sulfamide

There total 2 articles about N-(methoxycarbonylmethyl)-N'-[(2'S)-1,2-bis(benzyloxycarbonyl)ethyl]sulfamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1027892-86-9
C₂₆H₃₂N₂O₁₀S

: 249538-99-6
N-(methoxycarbonylmethyl)-N'-[(2'S)-1,2-bis(benzyloxycarbonyl)ethyl]sulfamide

Guidance literature:: With trifluoroacetic acid; In dichloromethane;

Reference yield:

: 1025873-02-2
C₂₃H₂₈N₂O₈S

: 249538-99-6
N-(methoxycarbonylmethyl)-N'-[(2'S)-1,2-bis(benzyloxycarbonyl)ethyl]sulfamide

Guidance literature:: Multi-step reaction with 2 steps

1: Ph₃P; diisopropyl diazodicarboxylate / tetrahydrofuran

2: 100 percent / trifluoroacetic acid / CH₂Cl₂

With di-isopropyl azodicarboxylate; triphenylphosphine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; 1: Alkylation / 2: Hydrolysis;