Technology Process of C28H36O4
There total 2 articles about C28H36O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine / diethyl ether / 6 h / 0 - 20 °C
2: sodium iodide; aluminum (III) chloride / acetonitrile; dichloromethane / 1 h / 0 - 20 °C
3: potassium carbonate; 1-methyl-3-methylimidazol-3-ium dimethyl phosphate / toluene / 0.83 h / 110 °C / Inert atmosphere; Microwave irradiation
With
aluminum (III) chloride; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; potassium carbonate; sodium iodide; 1-methyl-3-methylimidazol-3-ium dimethyl phosphate;
In
diethyl ether; dichloromethane; toluene; acetonitrile;
DOI:10.1021/jm3008213
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium iodide; aluminum (III) chloride / acetonitrile; dichloromethane / 1 h / 0 - 20 °C
2: potassium carbonate; 1-methyl-3-methylimidazol-3-ium dimethyl phosphate / toluene / 0.83 h / 110 °C / Inert atmosphere; Microwave irradiation
With
aluminum (III) chloride; potassium carbonate; sodium iodide; 1-methyl-3-methylimidazol-3-ium dimethyl phosphate;
In
dichloromethane; toluene; acetonitrile;
DOI:10.1021/jm3008213
- Guidance literature:
-
With
boron tribromide;
In
dichloromethane;
at -78 - 20 ℃;
for 24.5h;
Inert atmosphere;
DOI:10.1021/jm3008213