5-(N-allyl-2,2,2-trifluoroacetamido)-N,N'-bis-(2,3-dihydroxypropyl)-2,4,6-triiodoisophthalamide

Base Information

• Chemical Name: 5-(N-allyl-2,2,2-trifluoroacetamido)-N,N'-bis-(2,3-dihydroxypropyl)-2,4,6-triiodoisophthalamide
• CAS No.: 171897-75-9
• Molecular Formula: C₁₉H₂₁F₃I₃N₃O₇
• Molecular Weight: 841.1

Synonyms:5-(N-allyl-2,2,2-trifluoroacetamido)-N,N'-bis-(2,3-dihydroxypropyl)-2,4,6-triiodoisophthalamide

Chemical Property of 5-(N-allyl-2,2,2-trifluoroacetamido)-N,N'-bis-(2,3-dihydroxypropyl)-2,4,6-triiodoisophthalamide

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Technology Process of 5-(N-allyl-2,2,2-trifluoroacetamido)-N,N'-bis-(2,3-dihydroxypropyl)-2,4,6-triiodoisophthalamide

There total 2 articles about 5-(N-allyl-2,2,2-trifluoroacetamido)-N,N'-bis-(2,3-dihydroxypropyl)-2,4,6-triiodoisophthalamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

allyl bromide (106-95-6) + N,N'-bis(2,3-dihydroxypropyl)-2,4,6-triiodo-5-(2,2,2-trifluoroacetamido)isophthalamide (167630-07-1) → 5-(N-allyl-2,2,2-trifluoroacetamido)-N,N'-bis-(2,3-dihydroxypropyl)-2,4,6-triiodoisophthalamide (171897-75-9)

Guidance literature:

With potassium carbonate; In N,N-dimethyl acetamide; for 24h; Ambient temperature;

DOI:10.3891/acta.chem.scand.49-0737

Reference yield:

5-amino-N,N'-bis(2,3-dihydroxypropyl)-2,4,6-triiodoisophthalamide (76801-93-9) → 5-(N-allyl-2,2,2-trifluoroacetamido)-N,N'-bis-(2,3-dihydroxypropyl)-2,4,6-triiodoisophthalamide (171897-75-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 94 percent / DMAP / toluene / 24 h / 40 °C

2: 84 percent / K₂CO₃ / N,N-dimethyl-acetamide / 24 h / Ambient temperature

With dmap; potassium carbonate; In N,N-dimethyl acetamide; toluene;

DOI:10.3891/acta.chem.scand.49-0737

Reference yield: 94.0%

5-(N-allyl-2,2,2-trifluoroacetamido)-N,N'-bis-(2,3-dihydroxypropyl)-2,4,6-triiodoisophthalamide (171897-75-9) → 5--N,N'-bis(2,3-dihydroxypropyl)-2,4,6-triiodoisophthalamide (171897-76-0)

Guidance literature:

With Amberlite IRA-68; bromine; at 0 ℃;

DOI:10.3891/acta.chem.scand.49-0737

upstream raw materials:

allyl bromide

N,N'-bis(2,3-dihydroxypropyl)-2,4,6-triiodo-5-(2,2,2-trifluoroacetamido)isophthalamide

5-amino-N,N'-bis(2,3-dihydroxypropyl)-2,4,6-triiodoisophthalamide

Downstream raw materials:

5--N,N'-bis(2,3-dihydroxypropyl)-2,4,6-triiodoisophthalamide

5,5'-(N-acetyl-2-hydroxypropane-1,3-diyldiamino)bis

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