benzylphosphonofluoridic acid

Base Information

• Chemical Name: benzylphosphonofluoridic acid
• CAS No.: 55137-99-0
• Molecular Formula: C₇H₈FO₂P
• Molecular Weight: 174.111
• Mol file: 55137-99-0.mol

Synonyms:benzylphosphonofluoridic acid

Chemical Property of benzylphosphonofluoridic acid

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of benzylphosphonofluoridic acid

There total 6 articles about benzylphosphonofluoridic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.7%

sodium benzyl(1H-imidazol-1-yl)phosphinate → benzylphosphonofluoridic acid (55137-99-0)

Guidance literature:

With tetrabutyl ammonium fluoride; zinc(II) chloride; In tetrahydrofuran; at 60 ℃; for 12h;

DOI:10.1016/j.tetlet.2021.152917

Reference yield: 32.0%

diphenyl benzylphosphonate (10419-87-1) → benzylphosphonofluoridic acid (55137-99-0)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 0.5h;

DOI:10.1021/acs.orglett.1c01211

Reference yield:

di-P-fluoro-benzylphosphonate (41698-25-3) → benzylphosphonofluoridic acid (55137-99-0)

Guidance literature:

With benzylphosphonic acid; at 120 ℃;

upstream raw materials:

di-P-fluoro-benzylphosphonate

benzylphosphonic dichloride

benzylphosphonic acid

diphenyl benzylphosphonate