Technology Process of C34H33O5P
There total 6 articles about C34H33O5P which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
N,N-dimethyl-formamide;
at -10 - 20 ℃;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: sodium cyanide / water / 30 - 45 °C
2: hydrogenchloride / 20 °C
3: 1H-imidazole / dichloromethane / 25 - 30 °C
4: N-Bromosuccinimide / acetone / 0 - 40 °C
5: sodium hydrogencarbonate; sodium hypochlorite; N-benzyl-N,N,N-triethylammonium chloride; potassium bromide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / hexane / -10 - 20 °C
6: potassium carbonate / N,N-dimethyl-formamide / -10 - 20 °C
With
1H-imidazole; hydrogenchloride; sodium cyanide; sodium hypochlorite; N-Bromosuccinimide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; N-benzyl-N,N,N-triethylammonium chloride; sodium hydrogencarbonate; potassium carbonate; potassium bromide;
In
hexane; dichloromethane; water; N,N-dimethyl-formamide; acetone;
6: Wittig Reaction;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: N-Bromosuccinimide / acetone / 0 - 40 °C
2: sodium hydrogencarbonate; sodium hypochlorite; N-benzyl-N,N,N-triethylammonium chloride; potassium bromide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / hexane / -10 - 20 °C
3: potassium carbonate / N,N-dimethyl-formamide / -10 - 20 °C
With
sodium hypochlorite; N-Bromosuccinimide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; N-benzyl-N,N,N-triethylammonium chloride; sodium hydrogencarbonate; potassium carbonate; potassium bromide;
In
hexane; N,N-dimethyl-formamide; acetone;
3: Wittig Reaction;