5-benzenesulfonylamino-3-methyl-2-phenyl-[1,3,4]thiadiazolium betaine

Base Information

• Chemical Name: 5-benzenesulfonylamino-3-methyl-2-phenyl-[1,3,4]thiadiazolium betaine
• CAS No.: 37764-98-0
• Molecular Formula: C₁₅H₁₃N₃O₂S₂
• Molecular Weight: 331.419
• Mol file: 37764-98-0.mol

Synonyms:5-benzenesulfonylamino-3-methyl-2-phenyl-[1,3,4]thiadiazolium betaine

Chemical Property of 5-benzenesulfonylamino-3-methyl-2-phenyl-[1,3,4]thiadiazolium betaine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 5-benzenesulfonylamino-3-methyl-2-phenyl-[1,3,4]thiadiazolium betaine

There total 2 articles about 5-benzenesulfonylamino-3-methyl-2-phenyl-[1,3,4]thiadiazolium betaine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzenesulfonyl isothiocyanate (1424-53-9) + N-methylbenzothiohydrazide (21048-05-5) → 5-benzenesulfonylamino-3-methyl-2-phenyl-[1,3,4]thiadiazolium betaine (37764-98-0)

Guidance literature:

In toluene;

DOI:10.1007/BF00477454

Reference yield:

1-methyl-1-benzoylhydrazine (1483-24-5) + benzenesulfonyl isothiocyanate (1424-53-9) → 5-benzenesulfonylamino-3-methyl-2-phenyl-[1,3,4]thiadiazolium betaine (37764-98-0)

Guidance literature:

DOI:10.1016/S0040-4039(01)84978-9

Reference yield:

5-benzenesulfonylamino-3-methyl-2-phenyl-[1,3,4]thiadiazolium betaine (37764-98-0) → N-(N'-Benzoyl-N'-methyl-hydrazinocarbothioyl)-benzenesulfonamide (51127-97-0)

Guidance literature:

With potassium hydroxide; In ethanol;

DOI:10.1007/BF00477454

upstream raw materials:

1-methyl-1-benzoylhydrazine

benzenesulfonyl isothiocyanate

N-methylbenzothiohydrazide

Downstream raw materials:

N-(N'-Benzoyl-N'-methyl-hydrazinocarbothioyl)-benzenesulfonamide