(2E,4E,6E,8E,10E)-11-((S)-1-tert-Butoxycarbonyl-2-phenyl-ethylcarbamoyl)-undeca-2,4,6,8,10-pentaenoic acid

Base Information

Chemical Name:(2E,4E,6E,8E,10E)-11-((S)-1-tert-Butoxycarbonyl-2-phenyl-ethylcarbamoyl)-undeca-2,4,6,8,10-pentaenoic acid
CAS No.:192068-72-7
Molecular Formula:C₂₅H₂₉NO₅
Molecular Weight:423.509
Hs Code.:

Synonyms:(2E,4E,6E,8E,10E)-11-((S)-1-tert-Butoxycarbonyl-2-phenyl-ethylcarbamoyl)-undeca-2,4,6,8,10-pentaenoic acid

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Chemical Property of (2E,4E,6E,8E,10E)-11-((S)-1-tert-Butoxycarbonyl-2-phenyl-ethylcarbamoyl)-undeca-2,4,6,8,10-pentaenoic acid

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Technology Process of (2E,4E,6E,8E,10E)-11-((S)-1-tert-Butoxycarbonyl-2-phenyl-ethylcarbamoyl)-undeca-2,4,6,8,10-pentaenoic acid

There total 3 articles about (2E,4E,6E,8E,10E)-11-((S)-1-tert-Butoxycarbonyl-2-phenyl-ethylcarbamoyl)-undeca-2,4,6,8,10-pentaenoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 192068-71-6
C₄₁H₄₇NO₅Si

: 192068-72-7
(2E,4E,6E,8E,10E)-11-((S)-1-tert-Butoxycarbonyl-2-phenyl-ethylcarbamoyl)-undeca-2,4,6,8,10-pentaenoic acid

Guidance literature:: With hydrogen fluoride; In tetrahydrofuran; acetonitrile; Ambient temperature;
DOI:10.1002/anie.199711101

Reference yield:

: 3049-34-1,101417-68-9
(2E,4E,6E)octa-2,4,6-triene-1,8-dial

: 192068-72-7
(2E,4E,6E,8E,10E)-11-((S)-1-tert-Butoxycarbonyl-2-phenyl-ethylcarbamoyl)-undeca-2,4,6,8,10-pentaenoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / NaH / tetrahydrofuran / 3 h / Ambient temperature

2: 45 percent / NaH / tetrahydrofuran / 2 h / Ambient temperature

3: 85 percent / aq. HF / tetrahydrofuran; acetonitrile / Ambient temperature

With hydrogen fluoride; sodium hydride; In tetrahydrofuran; acetonitrile;
DOI:10.1002/anie.199711101

Reference yield:

: 192068-68-1
C₂₆H₂₈O₃Si

: 192068-72-7
(2E,4E,6E,8E,10E)-11-((S)-1-tert-Butoxycarbonyl-2-phenyl-ethylcarbamoyl)-undeca-2,4,6,8,10-pentaenoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 45 percent / NaH / tetrahydrofuran / 2 h / Ambient temperature

2: 85 percent / aq. HF / tetrahydrofuran; acetonitrile / Ambient temperature

With hydrogen fluoride; sodium hydride; In tetrahydrofuran; acetonitrile;
DOI:10.1002/anie.199711101