2-(4-nitrobenzylidene)-N-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)hydrazidecarbothioamide

Base Information

Chemical Name:2-(4-nitrobenzylidene)-N-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)hydrazidecarbothioamide
CAS No.:81812-50-2
Molecular Formula:C₂₂H₂₆N₄O₁₁S
Molecular Weight:554.535
Hs Code.:

Synonyms:2-(4-nitrobenzylidene)-N-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)hydrazidecarbothioamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(4-nitrobenzylidene)-N-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)hydrazidecarbothioamide

Chemical Property:

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Technology Process of 2-(4-nitrobenzylidene)-N-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)hydrazidecarbothioamide

There total 3 articles about 2-(4-nitrobenzylidene)-N-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)hydrazidecarbothioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 63128-98-3
4-(2',3',4',6'-tetra-O-acetyl-β-D-glucopyranosyl)-3-thiosemicarbazide

: 555-16-8
4-nitrobenzaldehdye

: 81812-50-2
2-(4-nitrobenzylidene)-N-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)hydrazidecarbothioamide

Guidance literature:: With acetic acid; In isopropyl alcohol; at 80 ℃; for 2h;
DOI:10.1016/j.bmcl.2008.11.070

Reference yield:

: 14152-97-7
2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl isothiocyanate

: 81812-50-2
2-(4-nitrobenzylidene)-N-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)hydrazidecarbothioamide

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine; hydrazine hydrate

2: ethanol; acetic acid

With pyridine; ethanol; hydrazine hydrate; acetic acid;

Reference yield:

: 572-09-8
2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide

: 81812-50-2
2-(4-nitrobenzylidene)-N-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)hydrazidecarbothioamide

Guidance literature:: Multi-step reaction with 3 steps

1: xylene

2: pyridine; hydrazine hydrate

3: ethanol; acetic acid

With pyridine; ethanol; hydrazine hydrate; acetic acid; xylene;