N-(2-(aminomethyl)-4-chlorophenyl)-2H-1,2,3-triazol-4-amine monohydrochloride

Base Information

Chemical Name:N-(2-(aminomethyl)-4-chlorophenyl)-2H-1,2,3-triazol-4-amine monohydrochloride
CAS No.:1611444-78-0
Molecular Formula:C₉H₁₀ClN₅*ClH
Molecular Weight:260.126
Hs Code.:

Synonyms:N-(2-(aminomethyl)-4-chlorophenyl)-2H-1,2,3-triazol-4-amine monohydrochloride

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Chemical Property of N-(2-(aminomethyl)-4-chlorophenyl)-2H-1,2,3-triazol-4-amine monohydrochloride

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Technology Process of N-(2-(aminomethyl)-4-chlorophenyl)-2H-1,2,3-triazol-4-amine monohydrochloride

There total 2 articles about N-(2-(aminomethyl)-4-chlorophenyl)-2H-1,2,3-triazol-4-amine monohydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1611444-59-7
N-[2-(aminomethyl)-4-chlorophenyl]-3-benzyltriazol-4-amine

: 1611444-78-0
N-(2-(aminomethyl)-4-chlorophenyl)-2H-1,2,3-triazol-4-amine monohydrochloride

Guidance literature:: N-[2-(aminomethyl)-4-chlorophenyl]-3-benzyltriazol-4-amine; With palladium on activated charcoal; hydrogen; zinc dibromide; In methanol; ethyl acetate; at 20 ℃; for 2h; Inert atmosphere;

With hydrogenchloride; In 1,4-dioxane; for 0.5h;

Reference yield:

: 1611444-60-0
2-[(3-benzyltriazol-4-yl)amino]-5-chlorobenzonitrile

: 1611444-78-0
N-(2-(aminomethyl)-4-chlorophenyl)-2H-1,2,3-triazol-4-amine monohydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: borane-THF / tetrahydrofuran / 1 h / 20 °C

1.2: 1 h

2.1: palladium on activated charcoal; hydrogen; zinc dibromide / methanol; ethyl acetate / 2 h / 20 °C / Inert atmosphere

2.2: 0.5 h

With borane-THF; palladium on activated charcoal; hydrogen; zinc dibromide; In tetrahydrofuran; methanol; ethyl acetate;