C₁₆H₁₇⁽²⁾H₅O₃S

Base Information

Chemical Name:C₁₆H₁₇⁽²⁾H₅O₃S
CAS No.:159145-88-7
Molecular Formula:C₁₆H₂₂O₃S
Molecular Weight:299.375
Hs Code.:

C<sub>16</sub>H<sub>17</sub><sup>(2)</sup>H<sub>5</sub>O<sub>3</sub>S

Synonyms:C₁₆H₁₇⁽²⁾H₅O₃S

Suppliers and Price of C₁₆H₁₇⁽²⁾H₅O₃S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₆H₁₇⁽²⁾H₅O₃S

Chemical Property:

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Technology Process of C₁₆H₁₇⁽²⁾H₅O₃S

There total 6 articles about C₁₆H₁₇⁽²⁾H₅O₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 98-59-9
p-toluenesulfonyl chloride

: 159145-87-6
(Z,Z)-3,6-nonadien-1-ol-8,9-d5

: 159145-88-7
C₁₆H₁₇⁽²⁾H₅O₃S

Guidance literature:: With pyridine; In dichloromethane; Ambient temperature;
DOI:10.1002/jlcr.2580340808

Reference yield:

: 159145-86-5
3,6-nonadiyn-1-ol-8,9-d5

: 159145-88-7
C₁₆H₁₇⁽²⁾H₅O₃S

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / 1.) H₂, NaBH₄, nickel acetate tetrahydrate, 2.) ethylenediamine / ethanol / 11 h / Ambient temperature

2: 81 percent / pyridine / CH₂Cl₂ / Ambient temperature

With pyridine; sodium tetrahydroborate; hydrogen; nickel diacetate; ethylenediamine; In ethanol; dichloromethane;
DOI:10.1002/jlcr.2580340808

Reference yield:

: 156673-68-6
C₁₀H₁₁⁽²⁾H₅O₂

: 159145-88-7
C₁₆H₁₇⁽²⁾H₅O₃S

Guidance literature:: Multi-step reaction with 6 steps

1: Dowex (H⁺) / methanol / 10 h

2: 91 percent / KOH / diethyl ether / 6 h / -50 - 20 °C

3: CuBr-dimethyl sulfide complex / tetrahydrofuran / 13 h / 0 - 20 °C

4: Dowex (H⁺) / methanol

5: 81 percent / 1.) H₂, NaBH₄, nickel acetate tetrahydrate, 2.) ethylenediamine / ethanol / 11 h / Ambient temperature

6: 81 percent / pyridine / CH₂Cl₂ / Ambient temperature

With pyridine; potassium hydroxide; sodium tetrahydroborate; copper(I) bromide dimethylsulfide complex; Dowex (H⁺); hydrogen; nickel diacetate; ethylenediamine; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane;
DOI:10.1002/jlcr.2580340808