methyl 4-bromo-2-{[(5-methoxy-2-methyl-1H-indol-3-yl)acetyl]amino) benzoate

Base Information

• Chemical Name: methyl 4-bromo-2-{[(5-methoxy-2-methyl-1H-indol-3-yl)acetyl]amino) benzoate
• CAS No.: 438535-18-3
• Molecular Formula: C₂₀H₁₉BrN₂O₄
• Molecular Weight: 431.286

Synonyms:methyl 4-bromo-2-{[(5-methoxy-2-methyl-1H-indol-3-yl)acetyl]amino) benzoate

Chemical Property of methyl 4-bromo-2-{[(5-methoxy-2-methyl-1H-indol-3-yl)acetyl]amino) benzoate

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Technology Process of methyl 4-bromo-2-{[(5-methoxy-2-methyl-1H-indol-3-yl)acetyl]amino) benzoate

There total 1 articles about methyl 4-bromo-2-{[(5-methoxy-2-methyl-1H-indol-3-yl)acetyl]amino) benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-Methoxy-2-methylindole-3-acetic acid (2882-15-7) + 2-amino-4-bromo-benzoic acid methyl ester (135484-83-2) → methyl 4-bromo-2-{[(5-methoxy-2-methyl-1H-indol-3-yl)acetyl]amino) benzoate (438535-18-3)

Guidance literature:

In tetrahydrofuran; cyclohexane;

Reference yield:

methyl 4-bromo-2-{[(5-methoxy-2-methyl-1H-indol-3-yl)acetyl]amino) benzoate (438535-18-3) + tert-Butyl acrylate (1663-39-4,25232-27-3) + tris-(o-tolyl)phosphine (6163-58-2) → 4-[(1E)-3-tert-butoxy-3-oxoprop-1-enyl]-2-{[(5-methoxy-2-methyl-1H-indol-3-yl)acetyl]amino}benzoic acid (438535-08-1)

Guidance literature:

With triethylamine; palladium diacetate; In N-methyl-acetamide;

Reference yield:

tetrakis(triphenylphosphine) palladium(0) (14221-01-3) + methyl 4-bromo-2-{[(5-methoxy-2-methyl-1H-indol-3-yl)acetyl]amino) benzoate (438535-18-3) + tetraethyltin (597-64-8) → 4-ethyl-2-{[(5-methoxy-2-methyl-1H-indol-3-yl)acetyl]amino}benzoic acid (438535-09-2)

Guidance literature:

With lithium hydroxide; In tetrahydrofuran; water; toluene;

upstream raw materials:

5-Methoxy-2-methylindole-3-acetic acid

2-amino-4-bromo-benzoic acid methyl ester

Downstream raw materials:

4-ethyl-2-{[(5-methoxy-2-methyl-1H-indol-3-yl)acetyl]amino}benzoic acid

4-[(1E)-3-tert-butoxy-3-oxoprop-1-enyl]-2-{[(5-methoxy-2-methyl-1H-indol-3-yl)acetyl]amino}benzoic acid

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