3,4,5-trimethoxy-2-(3,4-methylenedioxy-6-nitrophenyl)bromomethylbenzene

Base Information

Chemical Name:3,4,5-trimethoxy-2-(3,4-methylenedioxy-6-nitrophenyl)bromomethylbenzene
CAS No.:1407590-19-5
Molecular Formula:C₁₇H₁₆BrNO₇
Molecular Weight:426.221
Hs Code.:

Synonyms:3,4,5-trimethoxy-2-(3,4-methylenedioxy-6-nitrophenyl)bromomethylbenzene

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Chemical Property of 3,4,5-trimethoxy-2-(3,4-methylenedioxy-6-nitrophenyl)bromomethylbenzene

Chemical Property:

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Technology Process of 3,4,5-trimethoxy-2-(3,4-methylenedioxy-6-nitrophenyl)bromomethylbenzene

There total 6 articles about 3,4,5-trimethoxy-2-(3,4-methylenedioxy-6-nitrophenyl)bromomethylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1407590-18-4
C₁₇H₁₇NO₈

: 1407590-19-5
3,4,5-trimethoxy-2-(3,4-methylenedioxy-6-nitrophenyl)bromomethylbenzene

Guidance literature:: With phosphorus tribromide; In dichloromethane; at 0 - 20 ℃; for 0.75h;
DOI:10.2174/157017812802850276

Reference yield:

: 86-81-7
3,4,5-trimethoxy-benzaldehyde

: 1407590-19-5
3,4,5-trimethoxy-2-(3,4-methylenedioxy-6-nitrophenyl)bromomethylbenzene

Guidance literature:: Multi-step reaction with 4 steps

1: N-Bromosuccinimide / chloroform / 3 h / Reflux

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾

3: sodium tetrahydroborate / methanol / 0.25 h / 25 °C

4: phosphorus tribromide / dichloromethane / 0.75 h / 0 - 20 °C

With sodium tetrahydroborate; N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; phosphorus tribromide; In methanol; dichloromethane; chloroform; 2: |Stille Cross Coupling;
DOI:10.2174/157017812802850276

Reference yield:

: 35274-53-4
2-bromo-3,4,5-tri-methoxybenzaldehyde

: 1407590-19-5
3,4,5-trimethoxy-2-(3,4-methylenedioxy-6-nitrophenyl)bromomethylbenzene

Guidance literature:: Multi-step reaction with 3 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾

2: sodium tetrahydroborate / methanol / 0.25 h / 25 °C

3: phosphorus tribromide / dichloromethane / 0.75 h / 0 - 20 °C

With sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; phosphorus tribromide; In methanol; dichloromethane; 1: |Stille Cross Coupling;
DOI:10.2174/157017812802850276