3-{6-[5-(tert-butyl-diphenyl-silanyloxy)-3-methyl-pent-3-enyl]-5-methoxymethoxy-5-methyl-tetrahydro-pyran-2-yl}-3-methoxymethoxy-butyronitrile

Base Information

Chemical Name:3-{6-[5-(tert-butyl-diphenyl-silanyloxy)-3-methyl-pent-3-enyl]-5-methoxymethoxy-5-methyl-tetrahydro-pyran-2-yl}-3-methoxymethoxy-butyronitrile
CAS No.:936747-49-8
Molecular Formula:C₃₆H₅₃NO₆Si
Molecular Weight:623.905
Hs Code.:

3-{6-[5-(<i>tert</i>-butyl-diphenyl-silanyloxy)-3-methyl-pent-3-enyl]-5-methoxymethoxy-5-methyl-tetrahydro-pyran-2-yl}-3-methoxymethoxy-butyronitrile

Synonyms:3-{6-[5-(tert-butyl-diphenyl-silanyloxy)-3-methyl-pent-3-enyl]-5-methoxymethoxy-5-methyl-tetrahydro-pyran-2-yl}-3-methoxymethoxy-butyronitrile

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Chemical Property of 3-{6-[5-(tert-butyl-diphenyl-silanyloxy)-3-methyl-pent-3-enyl]-5-methoxymethoxy-5-methyl-tetrahydro-pyran-2-yl}-3-methoxymethoxy-butyronitrile

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Technology Process of 3-{6-[5-(tert-butyl-diphenyl-silanyloxy)-3-methyl-pent-3-enyl]-5-methoxymethoxy-5-methyl-tetrahydro-pyran-2-yl}-3-methoxymethoxy-butyronitrile

There total 3 articles about 3-{6-[5-(tert-butyl-diphenyl-silanyloxy)-3-methyl-pent-3-enyl]-5-methoxymethoxy-5-methyl-tetrahydro-pyran-2-yl}-3-methoxymethoxy-butyronitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 936747-60-3
3-{6-[5-(tert-butyl-diphenyl-silanyloxy)-3-methyl-pent-3-enyl]-5-methoxymethoxy-5-methyl-tetrahydro-pyran-2-yl}-3-hydroxy-butyronitrile

: 107-30-2
chloromethyl methyl ether

: 936747-49-8
3-{6-[5-(tert-butyl-diphenyl-silanyloxy)-3-methyl-pent-3-enyl]-5-methoxymethoxy-5-methyl-tetrahydro-pyran-2-yl}-3-methoxymethoxy-butyronitrile

Guidance literature:: With N-ethyl-N,N-diisopropylamine; potassium iodide; In dichloromethane;
DOI:10.1055/s-2007-967970

Reference yield:

: 936747-59-0
toluene-4-sulfonic acid 2-{6-[5-(tert-butyl-diphenyl-silanyloxy)-3-methyl-pent-3-enyl]-5-methoxymethoxy-5-methyl-tetrahydro-pyran-2-yl}-2-hydroxy-propyl ester

: 936747-49-8
3-{6-[5-(tert-butyl-diphenyl-silanyloxy)-3-methyl-pent-3-enyl]-5-methoxymethoxy-5-methyl-tetrahydro-pyran-2-yl}-3-methoxymethoxy-butyronitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / ethanol; H₂O / 70 °C

2: 96 percent / DIPEA; KI / CH₂Cl₂

With N-ethyl-N,N-diisopropylamine; potassium iodide; In ethanol; dichloromethane; water;
DOI:10.1055/s-2007-967970

Reference yield:

: 291765-46-3
(R)-2-{(2S,5S,6R)-6-[(E)-5-(tert-Butyl-diphenyl-silanyloxy)-3-methyl-pent-3-enyl]-5-methoxymethoxy-5-methyl-tetrahydro-pyran-2-yl}-propane-1,2-diol

: 936747-49-8
3-{6-[5-(tert-butyl-diphenyl-silanyloxy)-3-methyl-pent-3-enyl]-5-methoxymethoxy-5-methyl-tetrahydro-pyran-2-yl}-3-methoxymethoxy-butyronitrile

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / Et₃N / 20 °C

2: 91 percent / ethanol; H₂O / 70 °C

3: 96 percent / DIPEA; KI / CH₂Cl₂

With triethylamine; N-ethyl-N,N-diisopropylamine; potassium iodide; In ethanol; dichloromethane; water;
DOI:10.1055/s-2007-967970