2-(4-Aminophenyl)-3-[4-[2-(1-pyrrolidinyl)ethoxy]-benzyl]benzo[b]thiophene

Base Information

• Chemical Name: 2-(4-Aminophenyl)-3-[4-[2-(1-pyrrolidinyl)ethoxy]-benzyl]benzo[b]thiophene
• CAS No.: 215388-46-8
• Molecular Formula: C₂₇H₂₈N₂OS
• Molecular Weight: 428.598

Synonyms:2-(4-Aminophenyl)-3-[4-[2-(1-pyrrolidinyl)ethoxy]-benzyl]benzo[b]thiophene

Chemical Property of 2-(4-Aminophenyl)-3-[4-[2-(1-pyrrolidinyl)ethoxy]-benzyl]benzo[b]thiophene

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Technology Process of 2-(4-Aminophenyl)-3-[4-[2-(1-pyrrolidinyl)ethoxy]-benzyl]benzo[b]thiophene

There total 1 articles about 2-(4-Aminophenyl)-3-[4-[2-(1-pyrrolidinyl)ethoxy]-benzyl]benzo[b]thiophene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

2-(4-aminophenyl)benzo[b]thiophene-3-yl 4-[2-(1-pyrrolidinyl)ethoxy]phenyl ketone (215382-37-9) → 2-(4-Aminophenyl)-3-[4-[2-(1-pyrrolidinyl)ethoxy]-benzyl]benzo[b]thiophene (215388-46-8)

Guidance literature:

With triethanolamine; In tetrahydrofuran; SiO₂;

Reference yield: 91.0%

(5-oxo-pyrrolidin-2-yl)-acetic acid (64520-53-2) + 2-(4-Aminophenyl)-3-[4-[2-(1-pyrrolidinyl)ethoxy]-benzyl]benzo[b]thiophene (215388-46-8) → 3-[4-[2-(1-Pyrrolidinyl)ethoxy]benzyl]-2-[4-[1-oxo-2-(5-oxopyrrolidin-2-yl)ethyl]phenyl]-benzo[b]thiophene Oxalate

Guidance literature:

In methanol; chloroform; SiO₂;

Reference yield: 67.0%

(-)-2-oxo-4-thiazolidine carboxylic acid (19750-45-9) + 2-(4-Aminophenyl)-3-[4-[2-(1-pyrrolidinyl)ethoxy]-benzyl]benzo[b]thiophene (215388-46-8) → (R)-3-[4-[2-(1-Pyrrolidinyl)ethoxy]benzyl]-2-[4-[(2-oxothiazolidin-4-ylcarbonyl)amino]phenyl]-benzo[b]thiophene Oxalate (215387-52-3)

Guidance literature:

In methanol; chloroform; SiO₂;

upstream raw materials:

2-(4-aminophenyl)benzo[b]thiophene-3-yl 4-[2-(1-pyrrolidinyl)ethoxy]phenyl ketone

Downstream raw materials:

3-[4-[2-(1-Pyrrolidinyl)ethoxy]benzyl]-2-[4-(3-oxocyclopentylcarbonylamino)phenyl]benzo[b]thiophene Trifluoroacetate

(R)-3-[4-[2-(1-Pyrrolidinyl)ethoxy]benzyl]-2-[4-[(2-oxothiazolidin-4-ylcarbonyl)amino]phenyl]-benzo[b]thiophene Oxalate

3-[4-[2-(1-Pyrrolidinyl)ethoxy]benzyl]-2-[4-(5-oxopyrrolidin-2-ylcarbonylamino)phenyl]benzo[b]thiophene Oxalate

3-[4-[2-(1-Pyrrolidinyl)ethoxy]benzyl]-2-[4-[(2-oxoimidazolidin-4-ylcarbonyl)amino]phenyl]-benzo[b]thiophene Oxalate

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