(E)-S-3-((3-((2-(5-mercaptopentanoyl)hydrazono)methyl)-5-vinylphenoxy)methyl)benzyl ethanethioate

Base Information

Chemical Name:(E)-S-3-((3-((2-(5-mercaptopentanoyl)hydrazono)methyl)-5-vinylphenoxy)methyl)benzyl ethanethioate
CAS No.:1268158-15-1
Molecular Formula:C₂₄H₂₈N₂O₃S₂
Molecular Weight:456.63
Hs Code.:

Synonyms:(E)-S-3-((3-((2-(5-mercaptopentanoyl)hydrazono)methyl)-5-vinylphenoxy)methyl)benzyl ethanethioate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-S-3-((3-((2-(5-mercaptopentanoyl)hydrazono)methyl)-5-vinylphenoxy)methyl)benzyl ethanethioate

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Technology Process of (E)-S-3-((3-((2-(5-mercaptopentanoyl)hydrazono)methyl)-5-vinylphenoxy)methyl)benzyl ethanethioate

There total 12 articles about (E)-S-3-((3-((2-(5-mercaptopentanoyl)hydrazono)methyl)-5-vinylphenoxy)methyl)benzyl ethanethioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 98139-46-9
5-mercaptopentanoic acid hydrazide

: 1268158-12-8
S-3-((3-formyl-5-vinylphenoxy)methyl)benzyl ethanethioate

: 1268158-15-1
(E)-S-3-((3-((2-(5-mercaptopentanoyl)hydrazono)methyl)-5-vinylphenoxy)methyl)benzyl ethanethioate

Guidance literature:: With acetic acid; In methanol; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1002/anie.201004779

Reference yield:

: C₁₈H₁₈O₅S

: 1268158-15-1
(E)-S-3-((3-((2-(5-mercaptopentanoyl)hydrazono)methyl)-5-vinylphenoxy)methyl)benzyl ethanethioate

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-dimethyl-formamide / 3 h / 20 °C

2: acetic acid / methanol / 2 h / 20 °C / Inert atmosphere

With acetic acid; In methanol; N,N-dimethyl-formamide;
DOI:10.1002/anie.201004779

Reference yield:

: 116645-45-5
methyl 5-(acetylthio)pentanoate

: 1268158-15-1
(E)-S-3-((3-((2-(5-mercaptopentanoyl)hydrazono)methyl)-5-vinylphenoxy)methyl)benzyl ethanethioate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / methanol / Inert atmosphere; Reflux

2: acetic acid / methanol / 2 h / 20 °C / Inert atmosphere

With hydrazine hydrate; acetic acid; In methanol;
DOI:10.1002/anie.201004779