C₄₇H₆₄O₉

Base Information

Chemical Name:C₄₇H₆₄O₉
CAS No.:170707-15-0
Molecular Formula:C₄₇H₆₄O₉
Molecular Weight:773.02
Hs Code.:

C<sub>47</sub>H<sub>64</sub>O<sub>9</sub>

Synonyms:C₄₇H₆₄O₉

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Chemical Property of C₄₇H₆₄O₉

Chemical Property:

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Technology Process of C₄₇H₆₄O₉

There total 68 articles about C₄₇H₆₄O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 858346-40-4
C₄₉H₆₈O₉

: 170707-15-0
C₄₇H₆₄O₉

Guidance literature:: With Grubbs catalyst first generation; In dichloromethane; at 20 ℃; for 1.5h;
DOI:10.1021/ja051171c

Reference yield: 87.0%

: 889109-21-1
C₄₇H₆₂O₉

: 170707-15-0
C₄₇H₆₄O₉

Guidance literature:: With pyridine; potassium diazodicarboxylate; acetic acid; In methanol; at 20 ℃; for 3h;
DOI:10.1021/jo0603025

Reference yield:

: 858346-53-9
(2R,4aR,6R,7S,8aR,9aS,10aS)-6-(tert-Butyl-dimethyl-silanyloxy)-7-[(R)-3-(tert-butyl-dimethyl-silanyloxy)-2-methyl-propyl]-10a-methyl-2-phenyl-octahydro-1,3,8,10-tetraoxa-anthracene

: 170707-15-0
C₄₇H₆₄O₉

Guidance literature:: Multi-step reaction with 18 steps

1.1: H₂ / Pd(OH)2/C / ethyl acetate / 4 h

2.1: 77 percent / KH / tetrahydrofuran / 2 h / 35 °C

3.1: 100 percent / HMDS; TMSI / CH₂Cl₂ / 1 h / 0 °C

4.1: (COCl)2; DMSO; Et₃N / CH₂Cl₂ / -78 - 20 °C

5.1: tetrahydrofuran / 0.5 h / 0 °C

6.1: (COCl)2; DMSO; Et₃N / CH₂Cl₂ / -78 - 20 °C

7.1: NaHMDS / tetrahydrofuran / 0 °C

7.2: 298 mg / tetrahydrofuran / 1 h / 20 °C

8.1: 84 percent / DDQ; aq. NaHCO₃ / CH₂Cl₂ / 1.5 h / 45 °C

9.1: KH / tetrahydrofuran / 1 h / 0 °C

10.1: 176 mg / (PCy₃)2Cl₂Ru=CHPh / CH₂Cl₂ / 20 h / 20 °C

11.1: 95 percent / CSA / methanol; CH₂Cl₂ / 2.5 h / 0 °C

12.1: 95 percent / Bu₃P / dimethylformamide / 4 h / 20 °C

13.1: NCS / CCl₄; CH₂Cl₂ / 0.5 h / 20 °C

14.1: 30 percent / DTBMP; AgOTf; 4 Angstroem molecular sieves / CH₂Cl₂ / 2 h / -45 °C

15.1: TBAF / tetrahydrofuran / 20 h / 20 °C

16.1: CSA / CH₂Cl₂ / 1 h / 20 °C

16.2: HMDS; TMSI / CH₂Cl₂ / 1 h / 0 °C

16.3: AgOTf; 4 Angstroem molecular sieves / CH₂Cl₂; acetonitrile / 7 h / 30 °C

17.1: 83 percent / (PCy₃)2Cl₂Ru=CHPh / benzene / 5 h / 80 °C

18.1: 87 percent / KO₂CN=NCOOK; pyridine; AcOH / methanol / 3 h / 20 °C

With pyridine; N-chloro-succinimide; Grubbs catalyst first generation; 2,6-di-tert-butyl-4-methylpyridine; oxalyl dichloride; trimethylsilyl iodide; tributylphosphine; 4 A molecular sieve; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; hydrogen; silver trifluoromethanesulfonate; sodium hexamethyldisilazane; potassium diazodicarboxylate; potassium hydride; sodium hydrogencarbonate; acetic acid; dimethyl sulfoxide; triethylamine; 1,1,1,3,3,3-hexamethyl-disilazane; 2,3-dicyano-5,6-dichloro-p-benzoquinone; palladium dihydroxide; In tetrahydrofuran; methanol; tetrachloromethane; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; benzene; 4.1: Swern oxidation / 5.1: Grignard reaction / 6.1: Swern oxidation / 7.2: Wittig reaction;
DOI:10.1021/jo0603025