7-phenylhepta-5,6-dien-1-ol

Base Information

• Chemical Name: 7-phenylhepta-5,6-dien-1-ol
• CAS No.: 1416051-33-6
• Molecular Formula: C₁₃H₁₆O
• Molecular Weight: 188.269
• Mol file: 1416051-33-6.mol

Synonyms:7-phenylhepta-5,6-dien-1-ol

Chemical Property of 7-phenylhepta-5,6-dien-1-ol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of 7-phenylhepta-5,6-dien-1-ol

There total 1 articles about 7-phenylhepta-5,6-dien-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-hexyl-1-ol (928-90-5) + benzyl chloride (100-44-7) → 7-phenylhepta-5,6-dien-1-ol (1416051-33-6) + C13H16O

Guidance literature:

benzyl chloride; With dichloro bis(acetonitrile) palladium(II); caesium carbonate; XPhos; In acetonitrile; at 20 ℃; for 0.05h; Inert atmosphere; Schlenk technique;

5-hexyl-1-ol; In acetonitrile; at 85 ℃; for 24h; Inert atmosphere; Schlenk technique;

DOI:10.1021/ol5026712

Reference yield: 94.0%

7-phenylhepta-5,6-dien-1-ol (1416051-33-6) → 7-phenylhepta-5,6-dienal

Guidance literature:

7-phenylhepta-5,6-dien-1-ol; With oxalyl dichloride; dimethyl sulfoxide; In dichloromethane; at -78 ℃; for 1h; Inert atmosphere;

With triethylamine; In dichloromethane; at -78 - 20 ℃; Inert atmosphere;

DOI:10.1002/chem.201500273

Reference yield: 85.0%

7-phenylhepta-5,6-dien-1-ol (1416051-33-6) → tetrahydro-2-(2-phenylethenyl)-2H-pyran (70028-17-0)

Guidance literature:

With iron(III) trifluoroacetate; In 1,2-dichloro-ethane; at 30 ℃; for 10h; Inert atmosphere;

DOI:10.1021/ol303021d

upstream raw materials:

5-hexyl-1-ol

benzyl chloride

Downstream raw materials:

tetrahydro-2-(2-phenylethenyl)-2H-pyran