rac-1,2-epoxy-2-methyl-5-(p-methoxyphenyl)-pentane

Base Information

• Chemical Name: rac-1,2-epoxy-2-methyl-5-(p-methoxyphenyl)-pentane
• CAS No.: 544711-44-6
• Molecular Formula: C₁₃H₁₈O₂
• Molecular Weight: 206.285

Synonyms:rac-1,2-epoxy-2-methyl-5-(p-methoxyphenyl)-pentane

Chemical Property of rac-1,2-epoxy-2-methyl-5-(p-methoxyphenyl)-pentane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of rac-1,2-epoxy-2-methyl-5-(p-methoxyphenyl)-pentane

There total 2 articles about rac-1,2-epoxy-2-methyl-5-(p-methoxyphenyl)-pentane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

1-methoxy-4-(4-methylpent-4-en-1-yl)benzene (74672-06-3) → rac-1,2-epoxy-2-methyl-5-(p-methoxyphenyl)-pentane (544711-44-6)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; for 0.833333h; cooling;

DOI:10.1016/S0957-4166(03)00117-4

Reference yield:

4-methoxyphenethyl bromide (14425-64-0) → rac-1,2-epoxy-2-methyl-5-(p-methoxyphenyl)-pentane (544711-44-6)

Guidance literature:

Multi-step reaction with 2 steps

1.1: Mg / tetrahydrofuran / 0.5 h / Heating

1.2: 71 percent / tetrahydrofuran / 16 h

2.1: 55 percent / m-chloroperoxybenzoic acid / CH₂Cl₂ / 0.83 h / cooling

With magnesium; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane;

DOI:10.1016/S0957-4166(03)00117-4

Reference yield: 62.0%

rac-1,2-epoxy-2-methyl-5-(p-methoxyphenyl)-pentane (544711-44-6) → 2-methyl-5-(p-methoxyphenyl)pentanal + 1,2,3,4-tetrahydro-7-methoxy-1-methyl-1-naphthalenemethanol

Guidance literature:

With methylaluminum dichloride; In hexane; dichloromethane; at -78 ℃; for 0.5h;

DOI:10.1016/S0957-4166(03)00117-4

upstream raw materials:

1-methoxy-4-(4-methylpent-4-en-1-yl)benzene

4-methoxyphenethyl bromide

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 544711-44-6 rac-1,2-epoxy-2-methyl-5-(p-methoxyphenyl)-pentane

Send

Send

Metric Ton KG G Pound L ML

Send

Send