Technology Process of C18H17Cl4N
There total 8 articles about C18H17Cl4N which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
lithium aluminium tetrahydride;
In
tetrahydrofuran;
at 80 ℃;
for 3h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: titanium(IV) tetraethanolate / tetrahydrofuran / 12 h / 70 °C
2: L-Selectride / tetrahydrofuran / 3 h / 0 - 20 °C
3: hydrogenchloride / methanol / 3 h / 20 °C
4: toluene / 12 h / 130 °C
5: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / 80 °C
With
hydrogenchloride; titanium(IV) tetraethanolate; lithium aluminium tetrahydride; L-Selectride;
In
tetrahydrofuran; methanol; toluene;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: sodium hydroxide / water / 2 h / 20 °C
2: hydrogen; palladium 10% on activated carbon; diphenyl sulfide / methanol / 24 h / 25 °C / 760.05 Torr
3: titanium(IV) tetraethanolate / tetrahydrofuran / 12 h / 70 °C
4: L-Selectride / tetrahydrofuran / 3 h / 0 - 20 °C
5: hydrogenchloride / methanol / 3 h / 20 °C
6: toluene / 12 h / 130 °C
7: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / 80 °C
With
hydrogenchloride; titanium(IV) tetraethanolate; lithium aluminium tetrahydride; diphenyl sulfide; palladium 10% on activated carbon; hydrogen; L-Selectride; sodium hydroxide;
In
tetrahydrofuran; methanol; water; toluene;