C₄₀H₆₆N₂O₅Si

Base Information

Chemical Name:C₄₀H₆₆N₂O₅Si
CAS No.:848731-54-4
Molecular Formula:C₄₀H₆₆N₂O₅Si
Molecular Weight:683.06
Hs Code.:

C<sub>40</sub>H<sub>66</sub>N<sub>2</sub>O<sub>5</sub>Si

Synonyms:C₄₀H₆₆N₂O₅Si

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Chemical Property of C₄₀H₆₆N₂O₅Si

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Technology Process of C₄₀H₆₆N₂O₅Si

There total 15 articles about C₄₀H₆₆N₂O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 848731-61-3
C₃₂H₅₈N₂O₄Si

: 824-94-2
p-methoxybenzyl chloride

: 848731-54-4
C₄₀H₆₆N₂O₅Si

Guidance literature:: With sodium hexamethyldisilazane; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1021/ol050038m

Reference yield:

: C₁₉H₂₂N₂O₆S

: 848731-54-4
C₄₀H₆₆N₂O₅Si

Guidance literature:: Multi-step reaction with 14 steps

1.1: tetrahydrofuran; diethyl ether / -78 - -10 °C

2.1: 98 percent / KHMDS / tetrahydrofuran / -78 - 0 °C

3.1: aq. HF / acetonitrile / 20 °C

3.2: 87 percent / Et₃N / CH₂Cl₂ / -78 - 20 °C

4.1: 92 percent / 2,6-di-tert-butyl-4-methylpyridine; BCl₃ / CH₂Cl₂; heptane / 15 h / 20 °C

5.1: imidazole / acetonitrile

6.1: NaBH₄ / methanol

7.1: Et₃N / CH₂Cl₂

8.1: Na; naphthalene / 1,2-dimethoxy-ethane; tetrahydrofuran / -78 °C

9.1: NaBH₃CN; AcOH / acetonitrile / 20 °C

10.1: 75 percent / (PCy₃)2Cl₂Ru=CHPh / CH₂Cl₂ / 7 h / Heating

11.1: 93 percent / H₂ / Pd/C / ethyl acetate / 6 h / 20 °C

12.1: 83 percent / HCl / tetrahydrofuran; H₂O / 20 °C

13.1: 89 percent / NaHMDS / dimethylformamide / 20 °C

With 1H-imidazole; hydrogenchloride; sodium tetrahydroborate; 2,6-di-tert-butyl-4-methylpyridine; naphthalene; hydrogen fluoride; hydrogen; sodium hexamethyldisilazane; sodium; boron trichloride; potassium hexamethylsilazane; sodium cyanoborohydride; acetic acid; triethylamine; palladium on activated charcoal; Grubbs catalyst first generation; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; diethyl ether; n-heptane; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; acetonitrile; 1.1: Grignarg reaction / 2.1: Swern oxidation / 3.1: Wittig reaction;
DOI:10.1021/ol050038m

Reference yield:

: C₂₀H₂₄N₂O₅S

: 848731-54-4
C₄₀H₆₆N₂O₅Si

Guidance literature:: Multi-step reaction with 15 steps

1.1: O₃; NaHCO₃ / CH₂Cl₂; methanol / -78 °C

1.2: 90 percent / Me₂S / -78 - 20 °C

2.1: tetrahydrofuran; diethyl ether / -78 - -10 °C

3.1: 98 percent / KHMDS / tetrahydrofuran / -78 - 0 °C

4.1: aq. HF / acetonitrile / 20 °C

4.2: 87 percent / Et₃N / CH₂Cl₂ / -78 - 20 °C

5.1: 92 percent / 2,6-di-tert-butyl-4-methylpyridine; BCl₃ / CH₂Cl₂; heptane / 15 h / 20 °C

6.1: imidazole / acetonitrile

7.1: NaBH₄ / methanol

8.1: Et₃N / CH₂Cl₂

9.1: Na; naphthalene / 1,2-dimethoxy-ethane; tetrahydrofuran / -78 °C

10.1: NaBH₃CN; AcOH / acetonitrile / 20 °C

11.1: 75 percent / (PCy₃)2Cl₂Ru=CHPh / CH₂Cl₂ / 7 h / Heating

12.1: 93 percent / H₂ / Pd/C / ethyl acetate / 6 h / 20 °C

13.1: 83 percent / HCl / tetrahydrofuran; H₂O / 20 °C

14.1: 89 percent / NaHMDS / dimethylformamide / 20 °C

With 1H-imidazole; hydrogenchloride; sodium tetrahydroborate; 2,6-di-tert-butyl-4-methylpyridine; naphthalene; hydrogen fluoride; hydrogen; sodium hexamethyldisilazane; sodium; boron trichloride; potassium hexamethylsilazane; sodium cyanoborohydride; sodium hydrogencarbonate; ozone; acetic acid; triethylamine; palladium on activated charcoal; Grubbs catalyst first generation; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; diethyl ether; n-heptane; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; acetonitrile; 2.1: Grignarg reaction / 3.1: Swern oxidation / 4.1: Wittig reaction;
DOI:10.1021/ol050038m