N,N'-dimethyl-N,N'-diphenyl-tetradecanediamide

Base Information

Chemical Name:N,N'-dimethyl-N,N'-diphenyl-tetradecanediamide
CAS No.:941286-74-4
Molecular Formula:C₂₈H₄₀N₂O₂
Molecular Weight:436.638
Hs Code.:

Synonyms:N,N'-dimethyl-N,N'-diphenyl-tetradecanediamide

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Chemical Property of N,N'-dimethyl-N,N'-diphenyl-tetradecanediamide

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Technology Process of N,N'-dimethyl-N,N'-diphenyl-tetradecanediamide

There total 1 articles about N,N'-dimethyl-N,N'-diphenyl-tetradecanediamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 821-38-5
1,14-tetradecanedioic acid

: 100-61-8
N-methylaniline

: 941286-74-4
N,N'-dimethyl-N,N'-diphenyl-tetradecanediamide

Guidance literature:: 1,14-tetradecanedioic acid; With 2-chloro-1-methyl-pyridinium iodide; In acetonitrile; for 1h; Heating;

N-methylaniline; With triethylamine; In acetonitrile; for 12h; Further stages.; Heating;
DOI:10.1021/ol070582q

Reference yield: 32.0%

: 941286-74-4
N,N'-dimethyl-N,N'-diphenyl-tetradecanediamide

: 941286-75-5
N,N'-dimethyl-N,N'-diphenyl-1,8-tetradecanediamine

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; for 7h; Heating;
DOI:10.1021/ol070582q

Reference yield:

: 941286-74-4
N,N'-dimethyl-N,N'-diphenyl-tetradecanediamide

: C₆₄H₈₆N₄O₄

Guidance literature:: Multi-step reaction with 2 steps

1: 32 percent / LiAlH₄ / tetrahydrofuran / 7 h / Heating

2: 50 percent / triethyl orthoformate / propan-2-ol / Heating

With lithium aluminium tetrahydride; orthoformic acid triethyl ester; In tetrahydrofuran; isopropyl alcohol;
DOI:10.1021/ol070582q