bis[(E)-4-(heptyloxy)phenyl-4-(4-(6-hydroxyhexyloxy)-2-hydroxybenzylideneamino)benzoate]copper

Base Information

Chemical Name:bis[(E)-4-(heptyloxy)phenyl-4-(4-(6-hydroxyhexyloxy)-2-hydroxybenzylideneamino)benzoate]copper
CAS No.:1408090-15-2
Molecular Formula:C₆₆H₈₀CuN₂O₁₂
Molecular Weight:1156.91
Hs Code.:

Synonyms:bis[(E)-4-(heptyloxy)phenyl-4-(4-(6-hydroxyhexyloxy)-2-hydroxybenzylideneamino)benzoate]copper

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis[(E)-4-(heptyloxy)phenyl-4-(4-(6-hydroxyhexyloxy)-2-hydroxybenzylideneamino)benzoate]copper

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Technology Process of bis[(E)-4-(heptyloxy)phenyl-4-(4-(6-hydroxyhexyloxy)-2-hydroxybenzylideneamino)benzoate]copper

There total 9 articles about bis[(E)-4-(heptyloxy)phenyl-4-(4-(6-hydroxyhexyloxy)-2-hydroxybenzylideneamino)benzoate]copper which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1227625-51-5
(E)-4-(heptyloxy)phenyl 4-(4-(6-hydroxyhexyloxy)-2-hydroxybenzylideneamino)benzoate

: 142-71-2
copper diacetate

: 1408090-15-2
bis[(E)-4-(heptyloxy)phenyl-4-(4-(6-hydroxyhexyloxy)-2-hydroxybenzylideneamino)benzoate]copper

Guidance literature:: In methanol; for 5h; Reflux;
DOI:10.1016/j.ica.2012.12.001

Reference yield:

: 13037-86-0
4-heptyloxyphenol

: 1408090-15-2
bis[(E)-4-(heptyloxy)phenyl-4-(4-(6-hydroxyhexyloxy)-2-hydroxybenzylideneamino)benzoate]copper

Guidance literature:: Multi-step reaction with 4 steps

1.1: dmap / N,N-dimethyl-formamide; dichloromethane / 0 °C / Irradiation

1.2: 13 h / 0 - 20 °C

2.1: palladium 10% on activated carbon / tetrahydrofuran; ethanol / 24 h / 20 °C

3.1: ethanol / 6 h / Reflux

4.1: methanol / 5 h / Reflux

With dmap; palladium 10% on activated carbon; In tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.ica.2012.12.001

Reference yield:

: 123-31-9,8027-02-9
hydroquinone

: 1408090-15-2
bis[(E)-4-(heptyloxy)phenyl-4-(4-(6-hydroxyhexyloxy)-2-hydroxybenzylideneamino)benzoate]copper

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydroxide / butan-1-ol / 0.5 h / 20 °C / Inert atmosphere

1.2: 60 h / 100 °C

2.1: dmap / N,N-dimethyl-formamide; dichloromethane / 0 °C / Irradiation

2.2: 13 h / 0 - 20 °C

3.1: palladium 10% on activated carbon / tetrahydrofuran; ethanol / 24 h / 20 °C

4.1: ethanol / 6 h / Reflux

5.1: methanol / 5 h / Reflux

With dmap; palladium 10% on activated carbon; sodium hydroxide; In tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide; butan-1-ol;
DOI:10.1016/j.ica.2012.12.001