(S)-2-[((2-(2,6-dimethoxyphenoxy)ethyl)amino)methyl]-8-hydroxy-1,4-benzodioxane

Base Information

Chemical Name:(S)-2-[((2-(2,6-dimethoxyphenoxy)ethyl)amino)methyl]-8-hydroxy-1,4-benzodioxane
CAS No.:1416443-87-2
Molecular Formula:C₁₉H₂₃NO₆
Molecular Weight:361.395
Hs Code.:

Synonyms:(S)-2-[((2-(2,6-dimethoxyphenoxy)ethyl)amino)methyl]-8-hydroxy-1,4-benzodioxane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-2-[((2-(2,6-dimethoxyphenoxy)ethyl)amino)methyl]-8-hydroxy-1,4-benzodioxane

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Technology Process of (S)-2-[((2-(2,6-dimethoxyphenoxy)ethyl)amino)methyl]-8-hydroxy-1,4-benzodioxane

There total 2 articles about (S)-2-[((2-(2,6-dimethoxyphenoxy)ethyl)amino)methyl]-8-hydroxy-1,4-benzodioxane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 329966-51-0
(R)-2-iodomethyl-8-hydroxy-1,4-benzodioxane

: 40515-98-8
2-(2,6-dimethoxyphenoxy)ethylamine

: 1416443-87-2
(S)-2-[((2-(2,6-dimethoxyphenoxy)ethyl)amino)methyl]-8-hydroxy-1,4-benzodioxane

Guidance literature:: In isopropyl alcohol; for 20h; Reflux;
DOI:10.1016/j.ejmech.2012.09.049

Reference yield:

: 329966-20-3
(2R)-2-((tosyloxy)methyl)-8-hydroxy-1,4-benzodioxane

: 1416443-87-2
(S)-2-[((2-(2,6-dimethoxyphenoxy)ethyl)amino)methyl]-8-hydroxy-1,4-benzodioxane

Guidance literature:: Multi-step reaction with 2 steps

1: sodium iodide / acetone / 3 h / Reflux

2: isopropyl alcohol / 20 h / Reflux

With sodium iodide; In isopropyl alcohol; acetone;
DOI:10.1016/j.ejmech.2012.09.049