1,3-dipalmitoylglycerol 2-[17-(3-amino-2,4,6-triiodophenyl)heptadecanoate]

Base Information

Chemical Name:1,3-dipalmitoylglycerol 2-[17-(3-amino-2,4,6-triiodophenyl)heptadecanoate]
CAS No.:102831-76-5
Molecular Formula:C₅₈H₁₀₂I₃NO₆
Molecular Weight:1290.16
Hs Code.:

Synonyms:1,3-dipalmitoylglycerol 2-[17-(3-amino-2,4,6-triiodophenyl)heptadecanoate]

Suppliers and Price of 1,3-dipalmitoylglycerol 2-[17-(3-amino-2,4,6-triiodophenyl)heptadecanoate]

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,3-dipalmitoylglycerol 2-[17-(3-amino-2,4,6-triiodophenyl)heptadecanoate]

Chemical Property:

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Technology Process of 1,3-dipalmitoylglycerol 2-[17-(3-amino-2,4,6-triiodophenyl)heptadecanoate]

There total 4 articles about 1,3-dipalmitoylglycerol 2-[17-(3-amino-2,4,6-triiodophenyl)heptadecanoate] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 502-52-3
hexadecanoic acid, 2-hydroxy-1,3-propanediyl ester

: 102831-72-1
ω-(3-amino-2,4,6-triiodophenyl)heptadecanoic acid

: 102831-76-5
1,3-dipalmitoylglycerol 2-[17-(3-amino-2,4,6-triiodophenyl)heptadecanoate]

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; Ambient temperature;
DOI:10.1021/jm00159a019

Reference yield:

: 102831-66-3
methyl 17-(3-nitrophenyl)-16-heptadecenoate

: 102831-76-5
1,3-dipalmitoylglycerol 2-[17-(3-amino-2,4,6-triiodophenyl)heptadecanoate]

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / H₂ / 5percent Pd/C / ethanol / 4 h / 2327.2 Torr / Ambient temperature

2: 81 percent / ICl, 8 N aq. HCl / CHCl₃ / 3 h / 70 °C

3: 91 percent / NaOH / tetrahydrofuran; methanol / 3 h / Heating

4: 52 percent / dicyclohexylcarbodiimide (DCC), DMAP / CH₂Cl₂ / Ambient temperature

With hydrogenchloride; dmap; sodium hydroxide; hydrogen; Iodine monochloride; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; dichloromethane; chloroform;
DOI:10.1021/jm00159a019

Reference yield:

: 102831-68-5
methyl 17-(3-aminophenyl)heptadecanoate

: 102831-76-5
1,3-dipalmitoylglycerol 2-[17-(3-amino-2,4,6-triiodophenyl)heptadecanoate]

Guidance literature:: Multi-step reaction with 3 steps

1: 81 percent / ICl, 8 N aq. HCl / CHCl₃ / 3 h / 70 °C

2: 91 percent / NaOH / tetrahydrofuran; methanol / 3 h / Heating

3: 52 percent / dicyclohexylcarbodiimide (DCC), DMAP / CH₂Cl₂ / Ambient temperature

With hydrogenchloride; dmap; sodium hydroxide; Iodine monochloride; dicyclohexyl-carbodiimide; In tetrahydrofuran; methanol; dichloromethane; chloroform;
DOI:10.1021/jm00159a019