C₂₈H₂₄FNO₄

Base Information

Chemical Name:C₂₈H₂₄FNO₄
CAS No.:1373241-87-2
Molecular Formula:C₂₈H₂₄FNO₄
Molecular Weight:457.501
Hs Code.:

C<sub>28</sub>H<sub>24</sub>FNO<sub>4</sub>

Synonyms:C₂₈H₂₄FNO₄

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Chemical Property of C₂₈H₂₄FNO₄

Chemical Property:

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Technology Process of C₂₈H₂₄FNO₄

There total 8 articles about C₂₈H₂₄FNO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 1373241-86-1
C₂₈H₂₂FNO₄

: 1373241-87-2
C₂₈H₂₄FNO₄

Guidance literature:: With methanol; sodium tetrahydroborate; at 0 - 20 ℃; for 16h; Inert atmosphere;

Reference yield:

: 91-56-5,1186480-61-4,84788-92-1
indole-2,3-dione

: 1373241-87-2
C₂₈H₂₄FNO₄

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 °C

1.2: 3 h / 20 °C

2.1: isopropylmagnesium chloride / tetrahydrofuran / 1 h / 0 °C

2.2: 15 h / 0 - 20 °C

3.1: trifluoroacetic acid; triethylsilane / dichloromethane / 3 h / 0 - 10 °C

4.1: caesium carbonate / tetrahydrofuran / 0.5 h / 20 °C

4.2: 15 h / 20 °C

5.1: boron tribromide / dichloromethane / 0.5 h / -78 - 0 °C / Inert atmosphere

5.2: -40 °C

6.1: aluminum (III) chloride / dichloromethane / 48 h / 0 - 20 °C / Inert atmosphere

6.2: 0 °C

7.1: pyrrolidine / methanol / 0.5 h / 20 °C / Inert atmosphere

7.2: 16 h / Reflux; Inert atmosphere

8.1: sodium tetrahydroborate; methanol / 16 h / 0 - 20 °C / Inert atmosphere

With pyrrolidine; methanol; triethylsilane; aluminum (III) chloride; sodium tetrahydroborate; isopropylmagnesium chloride; boron tribromide; sodium hydride; caesium carbonate; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 459-46-1
4-Fluorobenzyl bromide

: 1373241-87-2
C₂₈H₂₄FNO₄

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 °C

1.2: 3 h / 20 °C

2.1: isopropylmagnesium chloride / tetrahydrofuran / 1 h / 0 °C

2.2: 15 h / 0 - 20 °C

3.1: trifluoroacetic acid; triethylsilane / dichloromethane / 3 h / 0 - 10 °C

4.1: caesium carbonate / tetrahydrofuran / 0.5 h / 20 °C

4.2: 15 h / 20 °C

5.1: boron tribromide / dichloromethane / 0.5 h / -78 - 0 °C / Inert atmosphere

5.2: -40 °C

6.1: aluminum (III) chloride / dichloromethane / 48 h / 0 - 20 °C / Inert atmosphere

6.2: 0 °C

7.1: pyrrolidine / methanol / 0.5 h / 20 °C / Inert atmosphere

7.2: 16 h / Reflux; Inert atmosphere

8.1: sodium tetrahydroborate; methanol / 16 h / 0 - 20 °C / Inert atmosphere

With pyrrolidine; methanol; triethylsilane; aluminum (III) chloride; sodium tetrahydroborate; isopropylmagnesium chloride; boron tribromide; sodium hydride; caesium carbonate; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;