Technology Process of C22H28O4
There total 7 articles about C22H28O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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Multi-step reaction with 2 steps
1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / tetrahydrofuran / 20 °C
2: sodium periodate / tetrahydrofuran; water
With
sodium periodate; osmium(VIII) oxide; 4-methylmorpholine N-oxide;
In
tetrahydrofuran; water;
DOI:10.1055/s-0030-1260586
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: oxalyl dichloride; dimethyl sulfoxide / -78 °C
2.1: diethyl ether / -78 - 20 °C
2.2: Reflux
3.1: potassium hydride / tetrahydrofuran; mineral oil / 0 - 20 °C
3.2: 0 - 20 °C
4.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / tetrahydrofuran / 20 °C
5.1: sodium periodate / tetrahydrofuran; water
With
sodium periodate; osmium(VIII) oxide; oxalyl dichloride; potassium hydride; dimethyl sulfoxide; 4-methylmorpholine N-oxide;
In
tetrahydrofuran; diethyl ether; water; mineral oil;
2.1: Brown's asymmetric alkylation / 2.2: Brown's asymmetric alkylation;
DOI:10.1055/s-0030-1260586