4-(tert-butyl)-N-((4-(tert-butyl)phenyl)sulfonyl)-N-fluorobenzenesulfonamide

Base Information

Chemical Name:4-(tert-butyl)-N-((4-(tert-butyl)phenyl)sulfonyl)-N-fluorobenzenesulfonamide
CAS No.:1355251-12-5
Molecular Formula:C₂₀H₂₆FNO₄S₂
Molecular Weight:427.561
Hs Code.:

Synonyms:4-(tert-butyl)-N-((4-(tert-butyl)phenyl)sulfonyl)-N-fluorobenzenesulfonamide

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Chemical Property of 4-(tert-butyl)-N-((4-(tert-butyl)phenyl)sulfonyl)-N-fluorobenzenesulfonamide

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Technology Process of 4-(tert-butyl)-N-((4-(tert-butyl)phenyl)sulfonyl)-N-fluorobenzenesulfonamide

There total 2 articles about 4-(tert-butyl)-N-((4-(tert-butyl)phenyl)sulfonyl)-N-fluorobenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.6%

: 1355251-10-3
4-tert-butyl-N-[(4-tert-butylphenyl)sulfonyl]benzenesulfonamide

: 1355251-12-5
4-(tert-butyl)-N-((4-(tert-butyl)phenyl)sulfonyl)-N-fluorobenzenesulfonamide

Guidance literature:: 4-tert-butyl-N-[(4-tert-butylphenyl)sulfonyl]benzenesulfonamide; With sodium hydroxide; In water; for 0.333333h;

With fluorine; In acetonitrile; at -30 - -20 ℃; Inert atmosphere;
DOI:10.1016/j.jfluchem.2011.10.012

Reference yield:

: 15084-51-2
4-tert-butylbenzenesulfonyl chloride

: C₁₀H₁₄FNO₂S

: 1355251-12-5
4-(tert-butyl)-N-((4-(tert-butyl)phenyl)sulfonyl)-N-fluorobenzenesulfonamide

Guidance literature:: C₁₀H₁₄FNO₂S; With sodium hydroxide; In methanol; at 20 ℃; for 0.5h;

4-tert-butylbenzenesulfonyl chloride; In methanol; at 0 - 20 ℃;
DOI:10.1021/acs.orglett.7b01599

Reference yield: 94.0%

: 1355251-12-5
4-(tert-butyl)-N-((4-(tert-butyl)phenyl)sulfonyl)-N-fluorobenzenesulfonamide

: C₂₃H₂₈O

: C₄₃H₅₃NO₃S

Guidance literature:: With pyridine; copper(l) cyanide; In dichloromethane; at 40 ℃; for 24h; regiospecific reaction; Inert atmosphere;
DOI:10.1021/acscatal.6b00759