C₃₅H₂₁BN₂O₂

Base Information

Chemical Name:C₃₅H₂₁BN₂O₂
CAS No.:1303477-79-3
Molecular Formula:C₃₅H₂₁BN₂O₂
Molecular Weight:512.375
Hs Code.:

C<sub>35</sub>H<sub>21</sub>BN<sub>2</sub>O<sub>2</sub>

Synonyms:C₃₅H₂₁BN₂O₂

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Chemical Property of C₃₅H₂₁BN₂O₂

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Technology Process of C₃₅H₂₁BN₂O₂

There total 7 articles about C₃₅H₂₁BN₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1303477-88-4
C₃₇H₂₇BF₂N₂O₂

: 1303477-79-3
C₃₅H₂₁BN₂O₂

Guidance literature:: With boron tribromide; In dichloromethane; at 0 - 20 ℃; for 4h;
DOI:10.1016/j.tet.2011.03.016

Reference yield:

: 658709-82-1
C₁₈H₂₂INO₄

: 1303477-79-3
C₃₅H₂₁BN₂O₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / N,N-dimethyl-formamide / 21.5 h / Reflux; Inert atmosphere

2.1: potassium hydroxide / ethylene glycol / 2 h / 160 °C / Inert atmosphere; Darkness

3.1: trifluoroacetic acid / dichloromethane / 20 h / Reflux; Inert atmosphere

3.2: 1 h / 20 °C / Inert atmosphere

3.3: 0.5 h / Reflux; Inert atmosphere

4.1: 2 h / 210 °C / Heating; Reduced pressure

5.1: boron tribromide / dichloromethane / 4 h / 0 - 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; boron tribromide; sodium carbonate; trifluoroacetic acid; potassium hydroxide; In dichloromethane; ethylene glycol; N,N-dimethyl-formamide; 1.1: Suzuki coupling;
DOI:10.1016/j.tet.2011.03.016

Reference yield:

: 1303477-72-6
C₁₇H₁₇NO

: 1303477-79-3
C₃₅H₂₁BN₂O₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: trifluoroacetic acid / dichloromethane / 20 h / Reflux; Inert atmosphere

1.2: 1 h / 20 °C / Inert atmosphere

1.3: 0.5 h / Reflux; Inert atmosphere

2.1: 2 h / 210 °C / Heating; Reduced pressure

3.1: boron tribromide / dichloromethane / 4 h / 0 - 20 °C

With boron tribromide; trifluoroacetic acid; In dichloromethane;
DOI:10.1016/j.tet.2011.03.016