p-toluenesulfonic acid dibutylphosphorylmethyl ester

Base Information

Chemical Name:p-toluenesulfonic acid dibutylphosphorylmethyl ester
CAS No.:630065-13-3
Molecular Formula:C₁₆H₂₇O₄PS
Molecular Weight:346.428
Hs Code.:

Synonyms:p-toluenesulfonic acid dibutylphosphorylmethyl ester

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Chemical Property of p-toluenesulfonic acid dibutylphosphorylmethyl ester

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Technology Process of p-toluenesulfonic acid dibutylphosphorylmethyl ester

There total 3 articles about p-toluenesulfonic acid dibutylphosphorylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 37016-74-3
di-n-butyl(hydroxymethyl)phosphinoxide

: 98-59-9
p-toluenesulfonyl chloride

: 630065-13-3
p-toluenesulfonic acid dibutylphosphorylmethyl ester

Guidance literature:: With potassium carbonate; In acetone; at 55 - 60 ℃; for 1h;
DOI:10.1134/S107036321809013X

Reference yield:

: 15754-54-8
dibutylphosphine oxide

: 630065-13-3
p-toluenesulfonic acid dibutylphosphorylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / cyclohexane / 48 h / 20 °C / Inert atmosphere

2: triethylamine / dichloromethane / 20 °C / Inert atmosphere

With potassium carbonate; triethylamine; In dichloromethane; cyclohexane;
DOI:10.1039/c2nj40330g

Reference yield:

: 50602-70-5
dibutylphosphinous acid

: 630065-13-3
p-toluenesulfonic acid dibutylphosphorylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydroxide / dimethyl sulfoxide; water / 1 h / 50 °C

2: potassium carbonate / acetone / 1 h / 55 - 60 °C

With potassium carbonate; potassium hydroxide; In water; dimethyl sulfoxide; acetone;
DOI:10.1134/S107036321809013X