6-(triethoxysilyl)hexyl 2-(((Methylthio)carbonothioyl)thio)-2-phenylacetate

Base Information

Chemical Name:6-(triethoxysilyl)hexyl 2-(((Methylthio)carbonothioyl)thio)-2-phenylacetate
CAS No.:1344059-17-1
Molecular Formula:C₂₂H₃₆O₅S₃Si
Molecular Weight:504.808
Hs Code.:

Synonyms:6-(triethoxysilyl)hexyl 2-(((Methylthio)carbonothioyl)thio)-2-phenylacetate

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Chemical Property of 6-(triethoxysilyl)hexyl 2-(((Methylthio)carbonothioyl)thio)-2-phenylacetate

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Technology Process of 6-(triethoxysilyl)hexyl 2-(((Methylthio)carbonothioyl)thio)-2-phenylacetate

There total 3 articles about 6-(triethoxysilyl)hexyl 2-(((Methylthio)carbonothioyl)thio)-2-phenylacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 75-15-0,12122-00-8
carbon disulfide

: 1344059-13-7
6-(triethoxysilyl)hexyl α-bromophenylacetate

: 5188-07-8
sodium thiomethoxide

: 1344059-17-1
6-(triethoxysilyl)hexyl 2-(((Methylthio)carbonothioyl)thio)-2-phenylacetate

Guidance literature:: carbon disulfide; sodium thiomethoxide; In diethyl ether; water; at 20 ℃; for 4h;

6-(triethoxysilyl)hexyl α-bromophenylacetate; In diethyl ether; water; at 20 ℃;
DOI:10.1021/ma202105y

Reference yield:

: 4870-65-9,31302-84-8
2-bromophenylacetic acid

: 1344059-17-1
6-(triethoxysilyl)hexyl 2-(((Methylthio)carbonothioyl)thio)-2-phenylacetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 24.5 h / 20 °C / Cooling with ice

2.1: platinum⁽⁰⁾-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex / toluene / 24 h / Inert atmosphere

3.1: diethyl ether; water / 4 h / 20 °C

3.2: 20 °C

With dmap; platinum⁽⁰⁾-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex; dicyclohexyl-carbodiimide; In diethyl ether; dichloromethane; water; toluene;
DOI:10.1021/ma202105y

Reference yield:

: 821-41-0
5-Hexen-1-ol

: 1344059-17-1
6-(triethoxysilyl)hexyl 2-(((Methylthio)carbonothioyl)thio)-2-phenylacetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 24.5 h / 20 °C / Cooling with ice

2.1: platinum⁽⁰⁾-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex / toluene / 24 h / Inert atmosphere

3.1: diethyl ether; water / 4 h / 20 °C

3.2: 20 °C

With dmap; platinum⁽⁰⁾-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex; dicyclohexyl-carbodiimide; In diethyl ether; dichloromethane; water; toluene;
DOI:10.1021/ma202105y