C₅₀H₆₁O₈SiClSi

Base Information

Chemical Name:C₅₀H₆₁O₈SiClSi
CAS No.:919770-72-2
Molecular Formula:C₅₀H₆₁ClO₈Si₂
Molecular Weight:881.654
Hs Code.:

C<sub>50</sub>H<sub>61</sub>O<sub>8</sub>SiClSi

Synonyms:C₅₀H₆₁O₈SiClSi

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Chemical Property of C₅₀H₆₁O₈SiClSi

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Technology Process of C₅₀H₆₁O₈SiClSi

There total 11 articles about C₅₀H₆₁O₈SiClSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 919770-71-1
C₅₀H₆₃O₉SiClSi

: 919770-72-2
C₅₀H₆₁O₈SiClSi

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; p-toluenesulfonyl chloride; In dichloromethane; at 23 ℃; for 1.83333h;
DOI:10.1021/ja0662467

Reference yield:

: 919770-67-5
C₃₈H₅₇BrO₅Si₂

: 919770-72-2
C₅₀H₆₁O₈SiClSi

Guidance literature:: Multi-step reaction with 7 steps

1.1: 75 percent / Cu(OAc)2 / tetrahydrofuran; pyridine / 0.3 h / 60 °C

2.1: 4 Angstroem molecular sieves / tetrahydrofuran; toluene / 0.25 h / 23 °C

2.2: lithium hexamethyldisilazide / tetrahydrofuran; toluene / 0.01 h / -78 °C

2.3: 30 percent / tert-butyllithium / tetrahydrofuran; toluene; pentane / -78 °C

3.1: triethylamine trihydrofluoride / acetonitrile / 13 h / -25 °C

4.1: 25.4 mg / N,N'-dicyclohexylcarbodiimide / tetrahydrofuran / 2.5 h / 0 °C

5.1: tetrabutylammonium fluoride; o-nitrophenol / tetrahydrofuran / 1.5 h / 0 °C

6.1: triethylamine / CH₂Cl₂ / 0.67 h / -78 °C

7.1: 20.8 mg / DABCO; p-toluenesulfonyl chloride / CH₂Cl₂ / 1.83 h / 23 °C

With 1,4-diaza-bicyclo[2.2.2]octane; copper diacetate; 4 A molecular sieve; triethylamine trihydrofluoride; tetrabutyl ammonium fluoride; triethylamine; p-toluenesulfonyl chloride; dicyclohexyl-carbodiimide; 2-hydroxynitrobenzene; In tetrahydrofuran; pyridine; dichloromethane; toluene; acetonitrile;
DOI:10.1021/ja0662467

Reference yield:

: 919770-68-6
C₃₈H₅₅BrO₅Si₂

: 919770-72-2
C₅₀H₆₁O₈SiClSi

Guidance literature:: Multi-step reaction with 6 steps

1.1: 4 Angstroem molecular sieves / tetrahydrofuran; toluene / 0.25 h / 23 °C

1.2: lithium hexamethyldisilazide / tetrahydrofuran; toluene / 0.01 h / -78 °C

1.3: 30 percent / tert-butyllithium / tetrahydrofuran; toluene; pentane / -78 °C

2.1: triethylamine trihydrofluoride / acetonitrile / 13 h / -25 °C

3.1: 25.4 mg / N,N'-dicyclohexylcarbodiimide / tetrahydrofuran / 2.5 h / 0 °C

4.1: tetrabutylammonium fluoride; o-nitrophenol / tetrahydrofuran / 1.5 h / 0 °C

5.1: triethylamine / CH₂Cl₂ / 0.67 h / -78 °C

6.1: 20.8 mg / DABCO; p-toluenesulfonyl chloride / CH₂Cl₂ / 1.83 h / 23 °C

With 1,4-diaza-bicyclo[2.2.2]octane; 4 A molecular sieve; triethylamine trihydrofluoride; tetrabutyl ammonium fluoride; triethylamine; p-toluenesulfonyl chloride; dicyclohexyl-carbodiimide; 2-hydroxynitrobenzene; In tetrahydrofuran; dichloromethane; toluene; acetonitrile;
DOI:10.1021/ja0662467