2-(3-O-benzyl-1,2-O-isopropylidene-α-D-xylo-tetrofuranos-4-yl)-4,4,5,5-tetramethyl-2-imidazoline 3-oxyde 1-oxyle

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Chemical Name:2-(3-O-benzyl-1,2-O-isopropylidene-α-D-xylo-tetrofuranos-4-yl)-4,4,5,5-tetramethyl-2-imidazoline 3-oxyde 1-oxyle
CAS No.:63658-89-9
Molecular Formula:C₂₁H₂₉N₂O₆
Molecular Weight:405.471
Hs Code.:

Synonyms:2-(3-O-benzyl-1,2-O-isopropylidene-α-D-xylo-tetrofuranos-4-yl)-4,4,5,5-tetramethyl-2-imidazoline 3-oxyde 1-oxyle

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Chemical Property of 2-(3-O-benzyl-1,2-O-isopropylidene-α-D-xylo-tetrofuranos-4-yl)-4,4,5,5-tetramethyl-2-imidazoline 3-oxyde 1-oxyle

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Technology Process of 2-(3-O-benzyl-1,2-O-isopropylidene-α-D-xylo-tetrofuranos-4-yl)-4,4,5,5-tetramethyl-2-imidazoline 3-oxyde 1-oxyle

There total 3 articles about 2-(3-O-benzyl-1,2-O-isopropylidene-α-D-xylo-tetrofuranos-4-yl)-4,4,5,5-tetramethyl-2-imidazoline 3-oxyde 1-oxyle which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 63522-00-9
2-(3-O-benzyl-1,2-O-isopropylidene-α-D-xylo-tetrofuranos-4-yl)-1,3-dihydroxy-4,4,5,5-tetramethylimidazolidine

: 39657-39-1
4,4,5,5-tetramethylimidazolin-1-oxyl-3-oxide

: 63658-89-9
2-(3-O-benzyl-1,2-O-isopropylidene-α-D-xylo-tetrofuranos-4-yl)-4,4,5,5-tetramethyl-2-imidazoline 3-oxyde 1-oxyle

Guidance literature:: With lead dioxide; In chloroform; for 2h; Ambient temperature;
DOI:10.1016/S0008-6215(00)85293-3

Reference yield:

: 14538-51-3,78375-92-5
2,3-bis(hydroxyamino)-2,3-dimethylbutane monosulfate

: 63658-89-9
2-(3-O-benzyl-1,2-O-isopropylidene-α-D-xylo-tetrofuranos-4-yl)-4,4,5,5-tetramethyl-2-imidazoline 3-oxyde 1-oxyle

Guidance literature:: Multi-step reaction with 2 steps

1: 54.4 percent / sodium acetate / methanol / 12 h / Ambient temperature

2: 76 percent / PbO₂ / CHCl₃ / 2 h / Ambient temperature

With sodium acetate; lead dioxide; In methanol; chloroform;
DOI:10.1016/S0008-6215(00)85293-3

Reference yield:

: 23558-05-6
3-O-benzyl-1,2-O-isopropylidene-1,5-D-xylo-dialdofuranose

: 63658-89-9
2-(3-O-benzyl-1,2-O-isopropylidene-α-D-xylo-tetrofuranos-4-yl)-4,4,5,5-tetramethyl-2-imidazoline 3-oxyde 1-oxyle

Guidance literature:: Multi-step reaction with 2 steps

1: 54.4 percent / sodium acetate / methanol / 12 h / Ambient temperature

2: 76 percent / PbO₂ / CHCl₃ / 2 h / Ambient temperature

With sodium acetate; lead dioxide; In methanol; chloroform;
DOI:10.1016/S0008-6215(00)85293-3