ethyl (Z)-2-(4-(p-tolyl)-1,3,4,5-tetrahydro-2H-benzo[b][1,4]diazepin-2-ylidene)acetate

Base Information

Chemical Name:ethyl (Z)-2-(4-(p-tolyl)-1,3,4,5-tetrahydro-2H-benzo[b][1,4]diazepin-2-ylidene)acetate
CAS No.:1533410-51-3
Molecular Formula:C₂₀H₂₂N₂O₂
Molecular Weight:322.407
Hs Code.:

Synonyms:ethyl (Z)-2-(4-(p-tolyl)-1,3,4,5-tetrahydro-2H-benzo[b][1,4]diazepin-2-ylidene)acetate

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Chemical Property of ethyl (Z)-2-(4-(p-tolyl)-1,3,4,5-tetrahydro-2H-benzo[b][1,4]diazepin-2-ylidene)acetate

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Technology Process of ethyl (Z)-2-(4-(p-tolyl)-1,3,4,5-tetrahydro-2H-benzo[b][1,4]diazepin-2-ylidene)acetate

There total 2 articles about ethyl (Z)-2-(4-(p-tolyl)-1,3,4,5-tetrahydro-2H-benzo[b][1,4]diazepin-2-ylidene)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: C₁₆H₁₈O₄

: 95-54-5
1,2-diamino-benzene

: 1533410-51-3
ethyl (Z)-2-(4-(p-tolyl)-1,3,4,5-tetrahydro-2H-benzo[b][1,4]diazepin-2-ylidene)acetate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In toluene; at 20 ℃; for 12h;
DOI:10.1055/s-0037-1609347

Reference yield: 77.0%

: 104-87-0
4-methyl-benzaldehyde

: 141-97-9
ethyl acetoacetate

: 95-54-5
1,2-diamino-benzene

: 1533410-51-3
ethyl (Z)-2-(4-(p-tolyl)-1,3,4,5-tetrahydro-2H-benzo[b][1,4]diazepin-2-ylidene)acetate

Guidance literature:: ethyl acetoacetate; 1,2-diamino-benzene; With dimethylbromosulphonium bromide; In 1,2-dichloro-ethane; at 20 ℃; for 0.25h;

4-methyl-benzaldehyde; In 1,2-dichloro-ethane; at 55 ℃; for 4h;
DOI:10.1055/s-0033-1338984